反应条件
1: 1.) KN(SiMe3)2 / 1.) THF, toluene, -78 deg C, 30 min, 2.) THF, toluene, from -78 deg C to 25 deg C
2: 1.) KHMDS / 1.) THF, -78 deg C, 30 min, 2.) THF, from -78 deg C to -30 deg C
3: 99 percent / ozone / CH2Cl2
View Scheme
参考文献
Dell'Erba, Carlo; Novi, Marino; Petrillo, Giovanni; Tavani, Cinzia
Tetrahedron, 1996 , vol. 52, # 16 p. 5889 - 5898
