2,2'-硫烷二基二[1-(4-氯苯基)乙酮]合成路线 (共 7 条)
反应条件
sodium sulfide in methanol T=20 - 60°C; 0.5 h;
参考文献
Drevko, B. I.; Zhukov, O. I.; Kharchenko, V. G.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 10 p. 1401 - 1404
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 10 p. 1548 - 1552
反应条件
1: AlCl3, aluminium chloride; bromine / methanol 2: sodium sulfide / ethanol View Scheme
参考文献
Su, Qiong; Zhao, Zi-Jian; Xu, Feng; Lou, Peng-Cai; Zhang, Kai; Xie, De-Xun; Shi, Lei; Cai, Qing-Yun; Peng, Zhi-Hong; An, De-Lie
European Journal of Organic Chemistry, 2013 , # 8 p. 1551 - 1557
反应条件
sodium sulfide; ethanol
参考文献
Miyahara,Y.
Journal of Heterocyclic Chemistry, 1979 , vol. 16, p. 1147 - 1151
反应条件
1: AlCl3 / CS2 2: aq. Na2S*9H2O / ethanol View Scheme
参考文献
Miyahara,Y.
Journal of Heterocyclic Chemistry, 1979 , vol. 16, p. 1147 - 1151
反应条件
Na2S*9H2O 0.25 h; Neat (no solvent)Grinding;
参考文献
Karade, Nandkishor N.; Tiwari, Girdharilal B.; Gampawar, Sumit V.; Shinde, Sandeep V.
Heteroatom Chemistry, 2009 , vol. 20, # 3 p. 172 - 176
参考文献
Chrzaszczewska; Chwalinski
Roczniki Chemii, vol. 7, p. 69,72
反应条件
titanium tetrachloride; zinc
McMurry coupling;
参考文献
Dang, Yizhe; Chen, Yi
European Journal of Organic Chemistry, 2007 , # 34 p. 5661 - 5664