1,3-二-2-噻吩基-2-丙烯醛基-1-酮合成路线 （共 6 条）
反应条件
1: thiophene-2-carbaldehyde With potassium hydroxide in methanol; water T=0°C; 0.166667 h; 2: 2-acetyl-thiophene in methanol; water T=0°C; 3 h;
参考文献
YEUNGNAM EDUCATIONAL FOUNDATION
Patent: WO2005/121129 A1, 2005 ;
Location in patent: Page/Page column 16 ;
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in tetrahydrofuran T=20°C; Sonogashira Cross-Coupling; 20 h; Inert atmosphereSchlenk technique;
参考文献
Teiber, Marco; Giebeler, Soenke; Lessing, Timo; Mueller, Thomas J. J.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 21 p. 3541 - 3552
反应条件
potassium hydroxide in ethanol
3 h; Heating;
参考文献
El-Rayyes, Nizar R.; Hovakeemian, George H.; Hmoud, Hayat S.
Journal of Chemical and Engineering Data, 1984 , vol. 29, # 2 p. 225 - 229
反应条件
hydrazine hydrate
0.25 h; Heating;
参考文献
El-Rayyes, Nizar R.; Hovakeemian, George H.; Hmoud, Hayat S.
Journal of Chemical and Engineering Data, 1984 , vol. 29, # 2 p. 225 - 229
反应条件
in diethyl ether; benzene
T=-5°C; 24 h;
参考文献
Dmitrieva,G.V. et al.
Journal of Organic Chemistry USSR (English Translation), 1977 , vol. 13, p. 1389 - 1394
Zhurnal Organicheskoi Khimii, 1977 , vol. 13, # 7 p. 1508 - 1513
参考文献
Al-Ghulikah
Asian Journal of Chemistry, 2012 , vol. 24, # 4 p. 1631 - 1637
