1,5-双(2-羟基苯氧基)乙醚合成路线 （共 15 条）
反应条件
1: 2,2'-(3-oxa-pentane-1,5-diyldioxy)bis(phenol) With caesium carbonate in acetonitrile 3 h; RefluxInert atmosphere; 2: diethylene glycol dimethanesulfonate in acetonitrile Inert atmosphereReflux;
参考文献
Hanes, Robert E.; Lee, Jong Chan; Ivy, Sheryl N.; Palka, Anna; Bartsch, Richard A.
Arkivoc, 2010 , vol. 2010, # 7 p. 238 - 248
反应条件
potassium hydroxide in dimethyl sulfoxide T=90°C; 2.5 h;
参考文献
Kotlyar; Gorodnyuk; Grigorash; Chuprin
Russian Journal of General Chemistry, 1998 , vol. 68, # 7 p. 1135 - 1138
反应条件
1: 2,2'-(3-oxa-pentane-1,5-diyldioxy)bis(phenol) With caesium carbonate in acetonitrile 3 h; RefluxInert atmosphere; 2: triethyleneglycol bismethanesulfonyl ester in acetonitrile Inert atmosphereReflux;
参考文献
Hanes, Robert E.; Lee, Jong Chan; Ivy, Sheryl N.; Palka, Anna; Bartsch, Richard A.
Arkivoc, 2010 , vol. 2010, # 7 p. 238 - 248
反应条件
1: 55 percent
2: 74 percent / FeCl3*6H2O, hydrazine monohydrate / charcoal / various solvent(s)
3: NaNO2, HCl / acetic acid; H2O
4: NaOH / H2O
5: 87 percent / K2CO3 / dimethylformamide / 4 h / 80 °C
View Scheme
参考文献
Shinkai, Seiji; Miyazaki, Kiminori; Manabe, Osamu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 449 - 456
反应条件
potassium hydroxide in ethanol; N,N-dimethyl-formamide
参考文献
Weber,E.; Voegtle,F.
Chemische Berichte, 1976 , vol. 109, p. 1803 - 1831
