2-溴-5-硝基-3-甲基吡啶合成路线 （共 3 条）
反应条件
phosphorus tribromide in N,N-dimethyl-formamide; toluene T=120°C; 0.333333 h; Inert atmosphereSealed tube;
参考文献
THE ROYAL INSTITUTION FOR THE ADVANCEMENT OF LEARNING/MCGILL UNIVERSITY; TSANTRIZOS, Youla, S.; DE SCHUTTER, Joris, Wim; LIN, Yih-Shyan
Patent: WO2011/147038 A1, 2011 ;
Location in patent: Page/Page column 57 ;
反应条件
iron; acetic acid in water T=40°C; 1 h;
参考文献
Duan, Maosheng; Kazmierski, Wieslaw M.; Chong, Pek Y.; DeAnda, Felix; Edelstein, Mark; Ferris, Rob; Peckham, Jennifer; Wheelan, Pat; Xiong, Zhiping; Zhang, Huichang; Nishizawa, Rena; Takaoka, Yoshikazu
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 21 p. 6470 - 6475
反应条件
hydrogen; palladium on activated charcoal in methanol
参考文献
WO2012/142329 A1, ;
Page/Page column 75 ;
WO 2012/142329 A1
