1-氯-4-(1,2-二溴乙基)苯合成路线 (共 9 条)
反应条件
Oxonereg;; NH4Br in water; acetonitrile T=20°C; 0.0333333 h; regioselective reaction;
参考文献
Agrawal, Manoj K.; Adimurthy, Subbarayappa; Ganguly, Bishwajit; Ghosh, Pushpito K.
Tetrahedron, 2009 , vol. 65, # 14 p. 2791 - 2797
反应条件
Oxonereg;; NH4Br in water; acetonitrile 13 h; Reflux;
参考文献
MacHarla, Arun Kumar; Chozhiyath Nappunni, Rohitha; Nama, Narender
Tetrahedron Letters, 2012 , vol. 53, # 11 p. 1401 - 1405
反应条件
Sodium bromate; sulfuric acid; sodium bromide in 1,4-dioxane; water T=20°C; 6.5 h;
参考文献
Patil, Rajendra D.; Joshi, Girdhar; Adimurthy, Subbarayappa; Ranu, Brindaban C.
Tetrahedron Letters, 2009 , vol. 50, # 21 p. 2529 - 2532
反应条件
sodium hypochlorite; potassium bromide in phosphate buffer; acetonitrile T=40°C; pH=10.4; 1 h;
参考文献
Klawonn, Markus; Bhor, Santosh; Mehltretter, Gerald; Doebler, Christian; Fischer, Christine; Beller, Matthias
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 3 p. 389 - 392
反应条件
sodium acetate in ethylene glycol dimethyl ether Kharash-Sosnovsky Allylic Oxidation; 12 h; RefluxGreen chemistry;
参考文献
Sawama, Yoshinari; Nakatani, Ryosuke; Imanishi, Takahiro; Fujiwara, Yuta; Monguchi, Yasunari; Sajiki, Hironao
RSC Advances, 2014 , vol. 4, # 17 p. 8657 - 8660
反应条件
carbon monoxide; bromine in dichloromethane 1.) 0 deg C, 0.5 h, 2.) 40 deg C, 0.5 h; Further byproducts given;
参考文献
Schmidt, Eckhart K.G.; Dogan, Mehmet
Journal of Organometallic Chemistry, 1982 , vol. 234, # 1 p. 73 - 84
反应条件
bromine in dichloromethane 1.) 0 deg C, 0.5 h, 2.) 40 deg C, 0.5 h; Further byproducts given;
参考文献
Schmidt, Eckhart K.G.; Dogan, Mehmet
Journal of Organometallic Chemistry, 1982 , vol. 234, # 1 p. 73 - 84
反应条件
indium; CoCl2.6H2O in methanol T=20°C; 1 h;
参考文献
Yoo, Byung Woo; Lee, Seok Joo; Park, Young Kwang; Choi, Ji Yong; Ahn, Young Sun
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 7 p. 1951 - 1952
参考文献
Patil, Rajendra D.; Adimurthy, Subbarayappa; Ranu, Brindaban C.
Synthetic Communications, 2010 , vol. 40, # 21 p. 3233 - 3239