3,5-二氯-4-羟基苯甲醛合成路线 （共 17 条）
反应条件
in methanol electrolysis at 0.13 mA/cm2, 1.4 F/mol, C.C.E. 906 --> 1111 mV vs SCE; electrolyte LiClO4; acidic conditions; Product distributionMechanism;
参考文献
Tetrahedron, , vol. 55, # 17 p. 5295 - 5302
反应条件
1: 3,5-dichloro-4-hydroxy-benzaldehyde With potassium carbonate in acetone T=20°C; 0.5 h; 2: methyl iodide in acetone T=20°C; Reflux;
参考文献
EXONHIT S.A.; LEBLOND, Bertrand; TAVERNE, Thierry; BEAUSOLEIL, Eric; CHAUVIGNAC, Cedric; CASAGRANDE, Anne-Sophie; DESIRE, Laurent
Patent: WO2011/151423 A1, 2011 ;
Location in patent: Page/Page column 175-176 ;
反应条件
sodium carbonate; potassium iodide in ethanol Heating;
参考文献
Hellot,J.-P. et al.
Chimica Therapeutica, 1970 , vol. 5, p. 55 - 64
反应条件
sulfuric acid; dihydrogen peroxide in methanol; water T=17 - 80°C; Dakin Reaction;
参考文献
MERCK PATENT GMBH; KADAM, Shahuraj Hanamantrao; PAKNIKAR, Shashikumar
Patent: WO2011/128018 A1, 2011 ;
Location in patent: Page/Page column 14 ;
参考文献
Dakin
American Chemical Journal, 1909 , vol. 42, p. 495
反应条件
sodium hydroxide; sodium tetrahydroborate
参考文献
Claus,P. et al.
Monatshefte fuer Chemie, 1972 , vol. 103, p. 1178 - 1193
参考文献
Papa et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 4906,4908
Full Text Show Details
Schering Int. Research Inst.
Patent: US2671802 , 1948 ;
