in neat (no solvent) heating in a closed tube at 130-135°C, 10 days;; traces of (CF3)2GeI2;;
参考文献
Clark; Willis
Journal of the American Chemical Society, 1962 , vol. 84, p. 898
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Gmelin Handbook: F: PerFHalOrg.4, 4.2.1, page 165 - 169
copper T=140°C; 20 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kobayashi, Yoshiro; Kumadaki, Itsumaro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 661 - 664
96 h; IrradiationThe yields, the kind of products depend on the time of the irrad. and/or the temp., and the mol. ratio. Other trifluorometh. agents investigated; Product distribution;
参考文献
Naumann,D.; Wilkes,B.
Journal of Fluorine Chemistry, 1985 , vol. 30, p. 73
