N,N-二乙基-2-氯乙酰胺合成路线 （共 70 条）
反应条件
T=150 - 170°C; P=760 Torr; 3 h;
参考文献
Zheltonogova, E. A.; Orlova, N. A.; Kobzareva, V. P.; Shipov, A. G.; Baukov, Yu. I.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 10 p. 2254 - 2262,2092 - 2099
反应条件
sodium iodide in acetone
48 h;
参考文献
Since, Marc; Terme, Thierry; Vanelle, Patrice
Tetrahedron, 2009 , vol. 65, # 31 p. 6128 - 6134
反应条件
T=165 - 170°C; P=160 - 200 Torr;
参考文献
Chauzov, V. A.; Studnev, Yu. N.; Iznoskova, M. G.; Fokin, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1987 , vol. 57, # 1 p. 110 - 113,93 - 95
反应条件
potassium hydroxide; potassium carbonate in benzene
6 h; Ambient temperatureother diarylphosphine oxides and dialkyl hydrogen phosphites, var. alkylating agents, var. reaction times, also in the presence 18-crown-6, and phase transfer catalysis; Product distribution;
参考文献
Petrov, K. A.; Sivova, L. I.; Smirnov, I. V.; Kryukova, L. Yu.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 2.1 p. 327 - 332,264 - 268
反应条件
potassium carbonate in acetonitrile
T=20°C; 5 h; Further byproducts given;
参考文献
Aladzheva, I. M.; Odinets, I. L.; Petrovskii, P. V.; Mastryukova, T. A.; Kabachnik, M. I.
Russian Journal of General Chemistry, 1993 , vol. 63, # 3.2 p. 431 - 437
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 3 p. 611 - 620
反应条件
potassium hydroxide; potassium carbonate in benzene
1 h; Ambient temperature;
参考文献
Petrov, K. A.; Sivova, L. I.; Smirnov, I. V.; Kryukova, L. Yu.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 2.1 p. 327 - 332,264 - 268
参考文献
Medved', T. Ya.; Chmutova, M. K.; Nesterova, N. P.; Koiro, O. E.; Kochetkova, N. E.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 9 p. 1743 - 1747
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , vol. 30, # 9 p. 2121 - 2127
反应条件
triethylamine
1.) benzene, reflux 2 h; 2.) benzene, reflux 1 h; Yield given. Multistep reaction;
参考文献
Chauzov, V. A.; Studnev, Yu. N.; Iznoskova, M. G.; Fokin, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1987 , vol. 57, # 1 p. 54 - 56,45 - 46
参考文献
Medved', T. Ya.; Chmutova, M. K.; Nesterova, N. P.; Koiro, O. E.; Kochetkova, N. E.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 9 p. 1743 - 1747
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , vol. 30, # 9 p. 2121 - 2127
参考文献
Medved', T. Ya.; Chmutova, M. K.; Nesterova, N. P.; Koiro, O. E.; Kochetkova, N. E.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 9 p. 1743 - 1747
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , vol. 30, # 9 p. 2121 - 2127
