1,1,1,3,3-五氯-丙烷合成路线 (共 81 条)
反应条件
hydrogen fluoride in sulfolane T=100°C; P=14480.5 Torr; 3 h;
参考文献
Atofina Chemicals, Inc.
Patent: US6362382 B1, 2002 ;
Location in patent: Page column 2 ;
反应条件
hydrogen fluoride; antimony(V) pentachloride T=65 - 70°C; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2006/58560 A1, 2006 ;
Location in patent: Page/Page column 3 ;
反应条件
T=200 - 500°C; Gas phase;
参考文献
Fukuju, Tadahiro; Yamamoto, Kikuo; Moriwaki, Masayuki; Komatsu, Yasutaka; Saito, Akihiro; Hosaka, Shunsuke; Tsunoda, Dai; Kawakami, Jun
Patent: US2012/53374 A1, 2012 ;
Location in patent: Page/Page column 9 ;
反应条件
hydrogen fluoride; fluorinated Cr2O3 T=275 - 335°C; P=863.483 Torr; Inert atmosphereGas phase; Product distribution / selectivity;
参考文献
HONEYWELL INTERNATIONAL INC.
Patent: US2012/172636 A1, 2012 ;
Location in patent: Page/Page column 4-5 ;
反应条件
hydrogen fluoride; titanium tetrachloride Product distribution / selectivity;
参考文献
HONEYWELL INTERNATIONAL INC.
Patent: US2012/172636 A1, 2012 ;
Location in patent: Page/Page column 5 ;
反应条件
1: With hydrogen fluoride; titanium tetrachloride T=20 - 120°C; P=18617.8 Torr; 1.16667 h; 2: With potassium hydroxide in water
参考文献
Honeywell International Business Machines
Patent: US6844475 B1, 2005 ;
Location in patent: Page column 3 ;
反应条件
hydrogen fluoride; chlorine; antimony(V) pentachloride T=80 - 95°C; P=8517.48 - 10069 Torr;
参考文献
Honeywell International, Inc.
Patent: US2005/90698 A1, 2005 ;
Location in patent: Page/Page column 5 ;
反应条件
1: With hydrogen fluoride; titanium tetrachloride T=90°C; P=10343.2 Torr; 2: With potassium hydroxide in water T=30°C;
参考文献
Central Glass Company, Limited
Patent: EP2341040 A1, 2011 ;
Location in patent: Page/Page column 14-15 ;
反应条件
hydrogen fluoride; SbF5 T=120 - 121°C; P=9551.8 - 29721.1 Torr; 3.5 h; Product distribution / selectivity;
参考文献
HONEYWELL INTERNATIONAL INC.; Nair, Haridasan K.; Singh, Rajiv Ratna; Poss, Andrew Joseph; Nalewajek, David
Patent: US2013/211156 A1, 2013 ;
Location in patent: Paragraph 0033; 0034 ;
反应条件
hydrogen fluoride; SbF5 T=120 - 121°C; P=9551.8 - 29721.1 Torr; 3.5 h; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2007/118003 A1, 2007 ;
Location in patent: Page/Page column 4-5 ;