1,1,1,3,3-五氯-丙烷合成路线 (共 81 条)
反应条件
hydrogen fluoride; SbF5
T=120 - 121°C; P=9551.8 - 29721.1 Torr; 3.5 h; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2007/118003 A1, 2007 ;
Location in patent: Page/Page column 4-5 ;
反应条件
hydrogen fluoride; Catalyst M-Chromium oxide
T=300°C;
参考文献
Honeywell International, Inc.
Patent: US2005/90698 A1, 2005 ;
Location in patent: Page/Page column 5 ;
反应条件
hydrogen fluoride
T=200 - 500°C; 0.00138889 - 0.00555556 h;
参考文献
HONEYWELL INTERNATIONAL INC.; Nair, Haridasan K.; Singh, Rajiv Ratna; Poss, Andrew Joseph; Nalewajek, David
Patent: US2013/211156 A1, 2013 ;
Location in patent: Paragraph 0035 ;
反应条件
hydrogen fluoride; SbF5
T=345°C; Product distribution; Further Variations:ReagentsTemperatures;
参考文献
Quan, Heng-Dao; Yang, Hui-E; Tamura, Masanori; Sekiya, Akira
Journal of Fluorine Chemistry, 2007 , vol. 128, # 3 p. 190 - 195
反应条件
hydrogen fluoride; TaClxFy
T=65 - 70°C; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2006/58560 A1, 2006 ;
Location in patent: Page/Page column 3 ;
反应条件
hydrogen fluoride; TiClxFy
T=30 - 70°C; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2006/58560 A1, 2006 ;
Location in patent: Page/Page column 3 ;
反应条件
hydrogen fluoride in sulfolane
T=100°C; P=14480.5 Torr; 3 h;
参考文献
Atofina Chemicals, Inc.
Patent: US6362382 B1, 2002 ;
Location in patent: Page column 2 ;
反应条件
anhydrous iron chloride; tri-N-butyl phosphate; iron
T=90 - 100°C; 5 h; Inert atmosphere; Product distribution / selectivity;
参考文献
Close, Joshua; Wang, Haiyou; Tung, Hsueh Sung
Patent: US2012/310021 A1, 2012 ;
Location in patent: Page/Page column 4 ;
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; pentacarbonyliron(0)
参考文献
Freidlina,R.Kh. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1977 , vol. 26, p. 151 - 154
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1977 , vol. 26, p. 174 - 177
反应条件
chlorine
T=80 - 100°C; Irradiation.mit UV-Licht;
参考文献
Davis; Whaley
Journal of the American Chemical Society, 1951 , vol. 73, p. 2361