4-氯-3-三氟甲基硫氰酸苯酯合成路线 （共 6 条）
反应条件
sodium hydrogencarbonate in dichloromethane; water T=0 - 20°C; 1.5 h;
参考文献
Tetrahedron Letters, , vol. 51, # 28 p. 3654 - 3657
反应条件
1: With 1,4-diaza-bicyclo[2.2.2]octane in toluene T=20°C; 8 h; 2: With bis(trichloromethyl) carbonate in dichloromethane T=-5°C; Reflux;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 9 p. 2923 - 2929
反应条件
in dichloromethane T=0 - 20°C; 1.75 h;
参考文献
WO2004/85425 A1, ;
Page 89 ;
WO 2004/085425 A1
反应条件
1: 1,4-diaza-bicyclo[2.2.2]octane / toluene 2: benzene-1,3,5-tricarboxylic acid / dichloromethane View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 21 p. 6549 - 6553,5
反应条件
benzene-1,3,5-tricarboxylic acid in dichloromethane
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 21 p. 6549 - 6553,5
反应条件
ammonia in water; acetone T=25 - 35°C; 6 h;
参考文献
DR. REDDY'S LABORATORIES LTD.; DR. REDDY'S LABORATORIES, INC.
Patent: WO2007/2461 A1, 2007 ;
Location in patent: Page/Page column 23 ;
WO 2007/002461 A1
