N-羟基-4-甲基苯甲酰胺合成路线 （共 16 条）
反应条件
N-bromosuccinmide; hydroxylamine hydrochloride; triphenylphosphine in triethylamine; acetonitrile T=20°C; Mitsunobu reaction; 2 h;
参考文献
Dhuru, Sameer P.; Salunkhe, Manikrao M.
Journal of the Chinese Chemical Society, 2000 , vol. 47, # 4 B p. 1007 - 1008
反应条件
potassium hydroxide; hydroxylamine in methanol T=20°C; pH=10; 12 h;
参考文献
Hoshino, Yujiro; Okuno, Moriaki; Kawamura, Eri; Honda, Kiyoshi; Inoue, Seiichi
Chemical Communications, 2009 , # 17 p. 2281 - 2283
反应条件
hydroxylamine hydrochloride; sodium hydrogencarbonate in water; ethyl acetate T=20°C; 0.0833333 h;
参考文献
Gao, Xi-Ai; Wang, Xian-Xue; Yan, Hao; Li, Jian; Yan, Ru-Long; Huang, Guo-Sheng
Journal of the Indian Chemical Society, 2013 , vol. 90, # 3 p. 381 - 385
反应条件
hydroxylamine hydrochloride; potassium hydroxide in methanol 24 h; Reflux;
参考文献
Kreye, Oliver; Wald, Sarah; Meier, Michael A. R.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 1 p. 81 - 86
反应条件
polymer-bound N-hydroxybenzenesulfonamide; sodium methylate in tetrahydrofuran; methanol T=20°C; Angeli-Rimini's reaction; 7 h;
参考文献
Porcheddu, Andrea; Giacomelli, Giampaolo
Journal of Organic Chemistry, 2006 , vol. 71, # 18 p. 7057 - 7059
反应条件
(hydroxy(tosyloxy)iodo)benzene in chloroform T=20 - 60°C; 2.16667 h;
参考文献
Ghosh, Harisadhan; Patel, Bhisma K.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 2 p. 384 - 390
反应条件
hydroxylamine in water; acetonitrile T=23°C; 14 h;
参考文献
Yoganathan, Sabesan; Miller, Scott J.
Organic Letters, 2013 , vol. 15, # 3 p. 602 - 605
反应条件
1: 90 percent / acetonitrile / 15 h / Ambient temperature 2: 95 percent / 120 °C View Scheme
参考文献
Yoganathan, Sabesan; Miller, Scott J.
Organic Letters, 2013 , vol. 15, # 3 p. 602 - 605
反应条件
dinitrogen tetraoxide in acetonitrile T=-20°C; 2 h;
参考文献
Tetrahedron Letters, , vol. 31, # 27 p. 3893 - 3894
反应条件
potassium carbonate in dimethyl sulfoxide T=90°C; Lossen rearrangement; 2 h;
参考文献
Hoshino, Yujiro; Okuno, Moriaki; Kawamura, Eri; Honda, Kiyoshi; Inoue, Seiichi
Chemical Communications, 2009 , # 17 p. 2281 - 2283
