(Z)-十六碳-7-烯基乙酸酯合成路线 (共 7 条)
反应条件
hydrogen; Lindlar's catalyst in hexane
参考文献
Kovalev,B.G.; Ishchenko,R.I.
Journal of Organic Chemistry USSR (English Translation), 1974 , vol. 10, p. 468 - 470
Zhurnal Organicheskoi Khimii, 1974 , vol. 10, # 3 p. 463 - 466
反应条件
1: H+
2: LAH / tetrahydrofuran / Ambient temperature
3: pyridine
View Scheme
参考文献
Tewari, Neera; Rohatgi, Amit; Bhushan, Kumar Hari; Subramanian, G. B. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 10 p. 851 - 855
反应条件
1: LAH / tetrahydrofuran / Ambient temperature
2: pyridine
View Scheme
参考文献
Tewari, Neera; Rohatgi, Amit; Bhushan, Kumar Hari; Subramanian, G. B. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 10 p. 851 - 855
反应条件
2: 1.) 9-borabicyclo<3.3.1>nonane (9-BBN), 2.) methanol, glacial acetic acid / 1.) THF, 0 deg C, 48 h, 2.) 25 deg C, 1 h
View Scheme
参考文献
Brown, Herbert C.; Wang, Kung K.
Journal of Organic Chemistry, 1986 , vol. 51, # 24 p. 4514 - 4517
反应条件
1: 85 percent / pyridine / Ambient temperature
3: 1.) 9-borabicyclo<3.3.1>nonane (9-BBN), 2.) methanol, glacial acetic acid / 1.) THF, 0 deg C, 48 h, 2.) 25 deg C, 1 h
View Scheme
参考文献
Brown, Herbert C.; Wang, Kung K.
Journal of Organic Chemistry, 1986 , vol. 51, # 24 p. 4514 - 4517
反应条件
2: 1.) 9-borabicyclo<3.3.1>nonane (9-BBN), 2.) methanol, glacial acetic acid / 1.) THF, 0 deg C, 48 h, 2.) 25 deg C, 1 h
View Scheme
参考文献
Brown, Herbert C.; Wang, Kung K.
Journal of Organic Chemistry, 1986 , vol. 51, # 24 p. 4514 - 4517
反应条件
pyridine
Yield given;
参考文献
Tewari, Neera; Rohatgi, Amit; Bhushan, Kumar Hari; Subramanian, G. B. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 10 p. 851 - 855