苯并[e][1]苯并呋喃合成路线 （共 30 条）
反应条件
1: 64 percent / thionyl chloride / dimethylformamide
2: 68 percent / 600 °C / 0.1 Torr / flash vacuum pyrolysis
View Scheme
参考文献
Hussain, Amjad; Parrick, John
Tetrahedron Letters, 1983 , vol. 24, # 6 p. 609 - 612
反应条件
in chloroform-d1
T=20°C; Isomerization; condensation; cyclization; dehydration; 48 h;
参考文献
Haselgrove, Thomas D.; Jevric, Martyn; Taylor, Dennis K.; Tiekink, Edward R. T.
Tetrahedron, 1999 , vol. 55, # 51 p. 14739 - 14762
反应条件
1: CH2Cl2 / 2 h
2: 76 percent / K2CO3 / dimethylformamide / 1.) 5 min, 2.) overnight
3: 59 percent / 0.33 h / 750 °C / 0 Torr
View Scheme
参考文献
Black, Michael; Cadogan; McNab, Hamish; MacPherson, Andrew D.; Roddam, V. Peter; Smith, Carol; Swenson, Helen R.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 17 p. 2483 - 2493
反应条件
1: 76 percent / K2CO3 / dimethylformamide / 1.) 5 min, 2.) overnight
2: 59 percent / 0.33 h / 750 °C / 0 Torr
View Scheme
参考文献
Black, Michael; Cadogan; McNab, Hamish; MacPherson, Andrew D.; Roddam, V. Peter; Smith, Carol; Swenson, Helen R.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 17 p. 2483 - 2493
反应条件
potassium carbonate
T=200°C;
参考文献
Hesse
Chemische Berichte, 1897 , vol. 30, p. 1438
Chemische Berichte, 1898 , vol. 31, p. 601 Anm.
反应条件
in chloroform-d1
T=20°C; Isomerization; condensation; cyclization; dehydration; 48 h;
参考文献
Haselgrove, Thomas D.; Jevric, Martyn; Taylor, Dennis K.; Tiekink, Edward R. T.
Tetrahedron, 1999 , vol. 55, # 51 p. 14739 - 14762
反应条件
in chloroform-d1
T=20°C; Isomerization; condensation; dehydration; 62 h;
参考文献
Haselgrove, Thomas D.; Jevric, Martyn; Taylor, Dennis K.; Tiekink, Edward R. T.
Tetrahedron, 1999 , vol. 55, # 51 p. 14739 - 14762
反应条件
acetic acid; zinc(II) chloride
参考文献
Stoermer
Justus Liebigs Annalen der Chemie, 1900 , vol. 312, p. 332
参考文献
Duro; Mazonne
Bollettino delle Sedute della Accademia Gioenia di Scienze Naturali in Catania, 1957 , vol. <4> 4, p. 61,64
反应条件
sodium acetate; acetic anhydride
参考文献
Emmott; Livingstone
Journal of the Chemical Society, 1957 , p. 3144,3147
