3-羟基-1,8-萘二甲酸酐合成路线 （共 7 条）
反应条件
potassium hydroxide T=120 - 220°C; 1.75 h;
参考文献
Brown, Roger F. C.; Coulston, Karen J.; Eastwood, Frank W.; Saminathan, Sugirtham
Australian Journal of Chemistry, 1987 , vol. 40, # 1 p. 107 - 120
反应条件
1: 75 percent / oleum / 95 °C 2: 79 percent / aq. KOH / 1.75 h / 120 - 220 °C View Scheme
参考文献
Australian Journal of Chemistry, , vol. 40, # 1 p. 107 - 120
反应条件
T=220 - 240°C; beim Verschmelzen;
参考文献
Chem. News J. Ind. Sci., , vol. 98, p. 279
Chem. Zentralbl., , vol. 80, # I p. 1876
反应条件
Ansaeuern und der waessr.Loesung der Schmelze;
参考文献
Chemische Berichte, , vol. 32, p. 3290
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, , vol. <5>14 II, p. 689
Gazzetta Chimica Italiana, , vol. 36, p. II,107
反应条件
ethanol; ammonia T=100°C;
参考文献
Zollinger
Helvetica Chimica Acta, 1950 , vol. 33, p. 530,537
反应条件
1: With sodium hydroxide in water T=100°C; 0.0166667 h; microwave irradiation; 2: With mercury(II) diacetate in water T=180°C; Pesci reaction; 0.25 h; microwave irradiation; 3: With hydrogenchloride in water T=120°C; 0.25 h; microwave irradiation; Title compound not separated from byproducts;
参考文献
Moseley, Jonathan D.; Gilday, John P.
Tetrahedron, 2006 , vol. 62, # 19 p. 4690 - 4697
反应条件
1: With sodium hydroxide in water
T=100°C; 0.0166667 h; microwave irradiation;
2: With mercury(II) diacetate in water
T=180°C; Pesci reaction; 0.25 h; microwave irradiation;
3: With hydrogenchloride in water
T=120°C; 0.25 h; microwave irradiation; Title compound not separated from byproducts;
参考文献
Moseley, Jonathan D.; Gilday, John P.
Tetrahedron, 2006 , vol. 62, # 19 p. 4690 - 4697
