(R)-(-)-1-苄氧基-3-(对甲苯磺酰氧基)-2-丙醇合成路线 （共 12 条）
反应条件
molecular s eves 3 Angstroem; boron trifluoride diethyl etherate in dichloromethane 1.) O deg C, 12 h; 2.) 20 deg C, 2 h;
参考文献
Byun, Hoe-Sup; Bittman, Robert
Tetrahedron Letters, 1989 , vol. 30, # 21 p. 2751 - 2754
反应条件
di(n-butyl)tin oxide; triethylamine in dichloromethane 4 h;
参考文献
Neimert-Andersson, Kristina; Blomberg, Eva; Somfai, Peter
Journal of Organic Chemistry, 2004 , vol. 69, # 11 p. 3746 - 3752
反应条件
boron trifluoride diethyl etherate in dichloromethane T=0°C;
参考文献
Journal of the American Chemical Society, , vol. 130, # 2 p. 412 - 413
反应条件
boron trifluoride diethyl etherate in dichloromethane T=4°C; 18 h; Yield given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 111, # 8 p. 3077 - 3079
反应条件
boron trifluoride diethyl etherate in dichloromethane T=4°C; 18 h; Yield given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 111, # 8 p. 3077 - 3079
反应条件
1.1: NaH / tetrahydrofuran / 0.5 h / 0 °C 1.2: 65 percent / tetrahydrofuran 2.1: 91 percent / Bu2SnO; Et3N / CH2Cl2 / 4 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 11 p. 3746 - 3752
反应条件
1: NaNO2, H2SO4 / 16 h / Ambient temperature 2: 70 percent / H+ 3: 83 percent / Ph3P, DEAD 4: 90 percent / LiAlH4 5: pyridine View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 40 p. 5505 - 5506
反应条件
1: 70 percent / H+ 2: 83 percent / Ph3P, DEAD 3: 90 percent / LiAlH4 4: pyridine View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 40 p. 5505 - 5506
反应条件
1: 83 percent / Ph3P, DEAD 2: 90 percent / LiAlH4 3: pyridine View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 40 p. 5505 - 5506
反应条件
1: 90 percent / LiAlH4 2: pyridine View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 40 p. 5505 - 5506
