4-甲基苯甲醛乙烷-1,2-二基二硫代缩醛合成路线 （共 16 条）
反应条件
POCl3 on montmorillonite in dichloromethane
T=20°C; 0.25 h;
参考文献
Jin, Tong-Shou; Sun, Guang; Li, Yan-Wei; Li, Tong-Shuang
Synthetic Communications, 2004 , vol. 34, # 22 p. 4105 - 4110
反应条件
2,4,6-trichloro-1,3,5-triazine in N,N-dimethyl-formamide
T=20°C; 1 h;
参考文献
Bandgar, Babasaheb P.; Joshi, Neeta S.; Bettigeri, Sampada V.
Monatshefte fur Chemie, 2007 , vol. 138, # 1 p. 67 - 71
反应条件
1: 90 percent / solid silica chloride / CH2Cl2 / 0.33 h / 20 °C
2: 96 percent / solid silica chloride / acetonitrile / 20 °C
3: 95 percent / solid silica chloride / CHCl3 / 0.25 h / 20 °C
View Scheme
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Hazarkhani, Hassan
Phosphorus, Sulfur and Silicon and the Related Elements, 2002 , vol. 177, # 12 p. 2847 - 2858
反应条件
1: 92 percent / solid silica chloride / CH2Cl2 / 0.25 h / 20 °C
2: 96 percent / solid silica chloride / acetonitrile / 20 °C
3: 95 percent / solid silica chloride / CHCl3 / 0.25 h / 20 °C
View Scheme
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Hazarkhani, Hassan
Phosphorus, Sulfur and Silicon and the Related Elements, 2002 , vol. 177, # 12 p. 2847 - 2858
反应条件
1: 96 percent / solid silica chloride / acetonitrile / 20 °C
2: 95 percent / solid silica chloride / CHCl3 / 0.25 h / 20 °C
View Scheme
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Hazarkhani, Hassan
Phosphorus, Sulfur and Silicon and the Related Elements, 2002 , vol. 177, # 12 p. 2847 - 2858
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) in diethyl ether; benzene
16 h; Heating;
参考文献
Tzeng, Yih-Ling; Yang, Ping-Fan; Mei, Nai-Wen; Yuan, Tien-Min; Yu, Chun-Chi; Luh, Tien-Yau
Journal of Organic Chemistry, 1991 , vol. 56, # 18 p. 5289 - 5293
