1,3-二甲基-2-苯基咪唑烷合成路线 （共 18 条）
反应条件
in benzene 6 h; Heating;
参考文献
Witek, Stanislaw; Bielawska, Alicja; Bielawski, Jacek
Polish Journal of Chemistry, 1982 , vol. 56, # 1 p. 207 - 212
反应条件
1: With naphthalene; lithium in tetrahydrofuran T=-40°C; 3 h; 2: With water in tetrahydrofuran T=-40°C; 0.5 h;
参考文献
Azzena, Ugo; Dettori, Giovanna; Pisano, Luisa; Siotto, Immacolata
Tetrahedron, 2005 , vol. 61, # 13 p. 3177 - 3182
反应条件
in chloroform-d1 12 h; Ambient temperature;
参考文献
Corriu, R. J. P.; Lanneau, Gerard F.; Mehta, V. D.
Journal of Organometallic Chemistry, 1991 , vol. 419, # 1 p. 9 - 26
参考文献
Moss, Robert A.; Cox, D. Phillip; Tomioka, Hideo
Tetrahedron Letters, 1984 , vol. 25, # 10 p. 1023 - 1026
反应条件
1: sodium tetrahydroborate / methanol / 20 - 70 °C / Inert atmosphere 2: THF-d8 (tetrahydrofuran-d8) / 600 h / phosphate buffer in D2O 3: THF-d8 (tetrahydrofuran-d8) / 600 h / phosphate buffer in D2O 4: THF-d8 (tetrahydrofuran-d8) / 240 h / phosphate buffer in D2O View Scheme
参考文献
Buchsnee Levrand, Barbara; Godin, Guillaume; Trachsel, Alain; De Saint Laumer, Jean-Yves; Lehn, Jean-Marie; Herrmann, Andreas
European Journal of Organic Chemistry, 2011 , # 4 p. 681 - 695
反应条件
1.1: 87 percent / p-toluenesulfonic acid / toluene / Heating 2.1: Li; naphthalene / tetrahydrofuran / 3 h / -40 °C 2.2: H2O / tetrahydrofuran / 0.5 h / -40 °C View Scheme
参考文献
Azzena, Ugo; Dettori, Giovanna; Pisano, Luisa; Siotto, Immacolata
Tetrahedron, 2005 , vol. 61, # 13 p. 3177 - 3182
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 1 h; Heating;
参考文献
Salerno, Alejandra; Ceriani, Vanina; Perillo, Isabel A.
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 7 p. 1725 - 1733
反应条件
1: pyridine-2-carboxylic acid; [Mn(ClO4)2]*6H2O; dihydrogen peroxide; sodium acetate / hexadeuterioacetone; water / 16 h / 0 - 20 °C 2: calcium chloride / diethyl ether / 20 °C View Scheme
参考文献
Pijper, Dirk; Saisaha, Pattama; De Boer, Johannes W.; Hoen, Rob; Smit, Christian; Meetsma, Auke; Hage, Ronald; Van Summeren, Ruben P.; Alsters, Paul L.; Feringa, Ben L.; Browne, Wesley R.
Dalton Transactions, 2010 , vol. 39, # 43 p. 10375 - 10381
反应条件
1: THF-d8 (tetrahydrofuran-d8) / 264 h / phosphate buffer in D2O 2: THF-d8 (tetrahydrofuran-d8) / 240 h / phosphate buffer in D2O View Scheme
参考文献
Buchsnee Levrand, Barbara; Godin, Guillaume; Trachsel, Alain; De Saint Laumer, Jean-Yves; Lehn, Jean-Marie; Herrmann, Andreas
European Journal of Organic Chemistry, 2011 , # 4 p. 681 - 695
反应条件
1: THF-d8 (tetrahydrofuran-d8) / 600 h / phosphate buffer in D2O 2: THF-d8 (tetrahydrofuran-d8) / 600 h / phosphate buffer in D2O 3: THF-d8 (tetrahydrofuran-d8) / 240 h / phosphate buffer in D2O View Scheme
参考文献
Buchsnee Levrand, Barbara; Godin, Guillaume; Trachsel, Alain; De Saint Laumer, Jean-Yves; Lehn, Jean-Marie; Herrmann, Andreas
European Journal of Organic Chemistry, 2011 , # 4 p. 681 - 695
