2,3,5,6-四氟茴香醚合成路线 （共 25 条）
反应条件
1: ethylene glycol dimethyl ether With sodium hydride in mineral oil; tert-butyl alcohol T=25°C; 1 h; 2: potassium (pentafluoro phenyl) trifluoro borate in mineral oil; tert-butyl alcohol T=30°C; 7 h;
参考文献
Journal of Fluorine Chemistry, , vol. 149, p. 82 - 87
反应条件
water; phosphorous acid trisdiethylamide in N,N-dimethyl-formamide T=20°C; protodebromination; 0.166667 h;
参考文献
Russian Chemical Bulletin, , vol. 46, # 4 p. 786 - 788
反应条件
methyl iodide in ammonia T=-40°C;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 5 p. 960 - 967
Zhurnal Organicheskoi Khimii, , vol. 20, # 5 p. 1055 - 1063
反应条件
dimethylphenylsilane; bis(1,2-diphenylphosphino)benzene; potassium tert-butylate; copper(l) chloride in tetrahydrofuran 12 h; Inert atmosphereReflux; regioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 11 p. 3203 - 3207
Angew. Chem., , vol. 125, # 11 p. 3285 - 3289,5
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 5 p. 960 - 967
Zhurnal Organicheskoi Khimii, , vol. 20, # 5 p. 1055 - 1063
反应条件
sodium methylate in methanol T=-58°C; Rate constant;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 778 - 780
参考文献
Tetrahedron, , vol. 27, p. 669 - 680
参考文献
Journal of Fluorine Chemistry, , vol. 15, p. 257 - 262
反应条件
in methanol; dimethylsulfoxide-d6 T=25°C; Kinetics;
参考文献
Tetrahedron Letters, , vol. 47, # 42 p. 7405 - 7407
反应条件
in methanol; dimethylsulfoxide-d6 T=25°C; Product distributionKinetics; Further Variations:SolventsTemperatures;
参考文献
Tetrahedron Letters, , vol. 47, # 42 p. 7405 - 7407
