2-邻苯二甲酰亚胺基乙酸甲酯合成路线 （共 28 条）
反应条件
tert.-butylhydroperoxide; copper(l) chloride in dichloromethane; water T=50°C; 24 h; Sealed tube;
参考文献
Yan, Xiaoyu; Fang, Kun; Liu, Hailan; Xi, Chanjuan
Chemical Communications, 2013 , vol. 49, # 90 p. 10650 - 10652
反应条件
in N,N-dimethyl-formamide T=80°C; 1 h;
参考文献
Takechi, Haruko; Machida, Minoru; Kanaoka,Yuichi
Liebigs Annalen der Chemie, 1986 , # 5 p. 859 - 868
反应条件
1: 1,3-dihydro-1,3-dioxo-2H-isoindole-2-acetic acid With 2,4,6-trichloro-1,3,5-triazine; potassium carbonate in tetrahydrofuran; acetonitrile T=0°C; 2.75 h; 2: diazomethane in diethyl ether T=0 - 20°C; 12 h;
参考文献
Forbes; Barrett; Lewis; Smith
Tetrahedron Letters, 2000 , vol. 41, # 51 p. 9943 - 9947
反应条件
sodium hydroxide; ozone T=-78°C; 3 h;
参考文献
Bower, Justin F.; Jumnah, Roshan; Williams, Andrew C.; Williams, Jonathan M. J.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 9 p. 1411 - 1420
反应条件
1: 73 percent / Ph3P / bis(dibenzylideneacetone)palladium / dimethylformamide / 19 h / 100 °C 2: 6 percent / ozone, 2.5 M NaOH / 3 h / -78 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 41 p. 6619 - 6622
反应条件
in dimethyl sulfoxide Irradiation;
参考文献
Tetrahedron Letters, , vol. 32, # 25 p. 2949 - 2950
反应条件
1: potassium carbonate / tetrahydrofuran / Cooling with ice 2: potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate / 1,1-dimethylpropan-1-ol / 24 h / 100 °C / 760.05 Torr View Scheme
参考文献
Chemical Communications, , vol. 47, # 44 p. 12074 - 12076
反应条件
1: thionyl chloride / 2 h / Reflux 2: potassium carbonate / tetrahydrofuran / Cooling with ice 3: potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate / 1,1-dimethylpropan-1-ol / 24 h / 100 °C / 760.05 Torr View Scheme
参考文献
Chemical Communications, , vol. 47, # 44 p. 12074 - 12076
反应条件
1: [bis(acetoxy)iodo]benzene; AZADO / dichloromethane; water / 1 h / 0 - 20 °C / |Inert atmosphere 2: diethyl ether / 1 h / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 14, # 19 p. 5010 - 5013
反应条件
in acetonitrile T=0°C; Irradiation;
参考文献
Tetrahedron Letters, , vol. 32, # 25 p. 2949 - 2950
