(S,S)-(-)-氢化苯偶姻合成路线 (共 230 条)
反应条件
sodium tetrahydroborate in water 0.025 h; microwave irradiation;
参考文献
Zeynizadeh, Behzad; Setamdideh, Davood
Journal of the Chinese Chemical Society, 2005 , vol. 52, # 6 p. 1179 - 1184
反应条件
osmium(VIII) oxide; cinchona alkaloid on mesoporous SBA-15 silica support T=0°C; 24 h;
参考文献
Lee, Hong Myung; Kim, Sang-Wook; Hyeon, Taeghwan; Kim, B. Moon
Tetrahedron Asymmetry, 2001 , vol. 12, # 11 p. 1537 - 1541
反应条件
anhydrous magnesium perchlorate; 3-(N,N-dimethylcarbamoyl)-1,2,4-trimethyl-1,4-dihydropyridine in acetonitrile-D3 T=0°C; 1 h; also with (S)-benzoin and opt. active dihydropyridine; stereoselectivity; Mechanism;
参考文献
Anju; Ramakrishnan; Thomas, Ajesh P.; Suresh, Eringathodi; Srinivasan, Alagar
Organic Letters, 2008 , vol. 10, # 24 p. 5545 - 5548
反应条件
dipotassium-1-silafluorene in tetrahydrofuran T=-78 - 20°C;
参考文献
Liu; Stringfellow; Ballweg; Guzei; West
Journal of the American Chemical Society, 2002 , vol. 124, # 1 p. 49 - 57
反应条件
N-methyl-2-indolinone; fluorous OsO4 in water; acetone; tert-butyl alcohol T=20°C; 36 h;
参考文献
Huang, Yangen; Meng, Wei-Dong; Qing, Feng-Ling
Tetrahedron Letters, 2004 , vol. 45, # 9 p. 1965 - 1968
反应条件
air; hydroquinone 1,4-phthalazinediyl diether; K2lt;OsO2(OH)4gt; in water; tert-butyl alcohol T=50°C; P=15001.2 Torr; pH=10.4; 24 h;
参考文献
Journal of Organometallic Chemistry, , vol. 621, # 1-2 p. 70 - 76
反应条件
in water; acetone; acetonitrile
参考文献
Council of Scientific and Industrial Research
Patent: US6552234 B1, 2003 ;
反应条件
air; 2,2'-thiobis(2,4-di-tert-butylphenol); triethylamine; copper(l) chloride in tetrahydrofuran T=20°C; 12 h;
参考文献
Angewandte Chemie - International Edition, , vol. 37, # 16 p. 2217 - 2220
反应条件
cadmium(II) sulphide in acetonitrile T=20°C; P=37.5038 Torr; 24 h; Inert atmosphereIrradiation;
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 17 p. 3556 - 3561
反应条件
N,N'-ethane-1,2-diyl-N,N'-[3,5-bis[3,5-bis(3,5-dimethoxybenzyloxy)benzyloxy]benzyloxy]-N,N,N',N'-tetramethylammonium dibromide; C120H134N2O28(2+)*O4Os(2-); water; 4-methylmorpholine N-oxide; (DHQ)2-PHAL in acetonitrile T=20°C; Sharpless asymmetric dihydroxylation; 0.5 h; Inert atmosphere; diastereoselective reaction;
参考文献
Fujita, Ken-Ichi; Yamazaki, Manabu; Ainoya, Taku; Tsuchimoto, Teruhisa; Yasuda, Hiroyuki
Tetrahedron, 2010 , vol. 66, # 44 p. 8536 - 8543