(S,S)-(-)-氢化苯偶姻合成路线 (共 230 条)
反应条件
tert.-butylhydroperoxide; osmium(VIII) oxide in water; toluene; acetonitrile T=0°C;
参考文献
Journal of Organic Chemistry, , vol. 59, # 6 p. 1375 - 1380
反应条件
magnesium in N,N-dimethyl-formamide T=20°C; 4 h;
参考文献
Uchida, Tetsuro; Kita, Yoshio; Maekawa, Hirofumi; Nishiguchi, Ikuzo
Tetrahedron, 2006 , vol. 62, # 13 p. 3103 - 3111
反应条件
titanium(IV) isopropylate in diethyl ether; dichloromethane T=0°C; 1 h; Title compound not separated from byproducts.;
参考文献
Muramatsu, Yusuke; Harada, Toshiro
Angewandte Chemie - International Edition, 2008 , vol. 47, # 6 p. 1088 - 1090
反应条件
titanium; chloro-trimethyl-silane; Ti(OPr)4 in ethylene glycol dimethyl ether 12 h; Heating;
参考文献
Fuerstner, Alois; Hupperts, Achim
Journal of the American Chemical Society, 1995 , vol. 117, # 16 p. 4468 - 4475
反应条件
2,2-dimethyl-1-propanenitrile; titanium(III) chloride; copper in dichloromethane T=-23°C; aldol reaction;
参考文献
Chemistry Letters, , # 11 p. 1157 - 1158
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran 0.25 h; Cooling with ice;
参考文献
Tetrahedron Asymmetry, , vol. 22, # 20-22 p. 1906 - 1917
反应条件
lt;V2Cl3(THF)6gt;2lt;Zn2Cl6gt; in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide T=20°C; 0.5 h;
参考文献
Tetrahedron Letters, , vol. 37, # 39 p. 7083 - 7086
反应条件
zinc(II) iodide; zinc in N,N-dimethyl-formamide T=70°C; 24 h;
参考文献
Chemical Communications, , # 24 p. 3048 - 3049
反应条件
K3Fe(CN)6; potassium carbonate in tbutanol-water; acetonitrile
反应条件
titanium(IV) isopropylate in diethyl ether; dichloromethane T=0°C; 1 h; Title compound not separated from byproducts.;
参考文献
Muramatsu, Yusuke; Harada, Toshiro
Angewandte Chemie - International Edition, 2008 , vol. 47, # 6 p. 1088 - 1090