(S,S)-(-)-氢化苯偶姻合成路线 （共 230 条）
反应条件
titanium(IV) isopropylate in diethyl ether; dichloromethane T=0°C; 1 h; Title compound not separated from byproducts.;
参考文献
Muramatsu, Yusuke; Harada, Toshiro
Angewandte Chemie - International Edition, 2008 , vol. 47, # 6 p. 1088 - 1090
反应条件
cadmium(II) sulphide in acetonitrile T=-15°C; P=37.5038 Torr; 24 h; Inert atmosphereIrradiation;
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 17 p. 3556 - 3561
反应条件
cadmium(II) sulphide in acetonitrile T=20°C; P=37.5038 Torr; 24 h; Inert atmosphereIrradiation;
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 17 p. 3556 - 3561
反应条件
sodium hydroxide; aluminium in methanol; water pinacol coupling; 0.0833333 h; microwave irradiation;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 45, # 1 p. 332 - 334
反应条件
cerium; iodine in tetrahydrofuran T=25°C; 1 h;
参考文献
Journal of Organometallic Chemistry, , vol. 299, p. 179 - 186
反应条件
1: 3-iodoprop-1-ene With chromium dichloride; H2Salen; triethylamine in acetonitrile T=20°C; Metallation; 2: benzaldehyde With chloro-trimethyl-silane in acetonitrile Addition;
参考文献
Angewandte Chemie - International Edition, , vol. 38, # 22 p. 3357 - 3359
反应条件
2,2-dimethyl-1-propanenitrile; titanium(III) chloride in dichloromethane T=20°C; aldol reaction;
参考文献
Chemistry Letters, , # 11 p. 1157 - 1158
反应条件
1: n-butyl-magnesium chloride With titanium(IV) isopropylate in dichloromethane T=-78°C; 0.166667 h; Inert atmosphere; 2: benzaldehyde With (R)-3-(3,5-diphenylphenyl)-2,2'-dihydroxy-1,1'-binaphthyl in diethyl ether; dichloromethane T=0°C; 3 h; Inert atmosphere; 3: With hydrogenchloride; water in diethyl ether; dichloromethane T=0°C; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 83, # 1 p. 19 - 32
反应条件
1: 3-chloroprop-1-ene With chromium dichloride; H2Salen; triethylamine in acetonitrile T=20°C; Metallation; 2: benzaldehyde With chloro-trimethyl-silane in acetonitrile Addition;
参考文献
Angewandte Chemie - International Edition, , vol. 38, # 22 p. 3357 - 3359
反应条件
2,2-dimethyl-1-propanenitrile; titanium(III) chloride; copper in dichloromethane T=0°C; Reformatsky reaction; 12 h; Title compound not separated from byproducts;
参考文献
Mukaiyama, Teruaki; Kagayama, Akifumi; Igarashi, Koji; Shiina, Isamu
Chemistry Letters, 1999 , # 11 p. 1157 - 1158
