(2-噻吩基甲基)三苯基溴化膦合成路线 （共 9 条）
反应条件
in toluene Substitution; 4 h; Heating;
参考文献
Aitken, R. Alan; Drysdale, Martin J.; Hill, Lawrence; Lumbard, Keith W.; Maccallum, James R.; Seth, Shirley
Tetrahedron, 1999 , vol. 55, # 36 p. 11039 - 11050
反应条件
in chloroform 1 h; Heating;
参考文献
Zhang, Jian-Xin; Dubois, Philippe; Jerome, Robert
Synthetic Communications, 1996 , vol. 26, # 16 p. 3091 - 3095
反应条件
1: NaBH4 View Scheme
参考文献
Liu, Zhi-Qiang; Fang, Qi; Wang, Dong; Cao, Du-Xia; Xue, Gang; Yu, Wen-Tao; Lei, Hong
Chemistry - A European Journal, 2003 , vol. 9, # 20 p. 5074 - 5084
反应条件
1: 0.134 g / benzoyl peroxide; N-bromosuccinimide / 1,2-dichloro-ethane / 1 h / Heating 2: 50 percent / benzene / 12 h / Heating View Scheme
参考文献
Ngwendson, Julius N.; Atemnkeng, Walters N.; Schultze, Cassandra M.; Banerjee, Anamitro
Organic Letters, 2006 , vol. 8, # 18 p. 4085 - 4088
参考文献
Hebbar, Nordine; Ramondenc, Yvan; Ple, Gerard; Dupas, Georges; Ple, Nelly
Tetrahedron, 2009 , vol. 65, # 21 p. 4190 - 4200
反应条件
potassium tert-butylate in acetonitrile T=20°C; 2 h;
参考文献
Ngwendson, Julius N.; Schultze, Cassandra M.; Bollinger, Jordan W.; Banerjee, Anamitro
Canadian Journal of Chemistry, 2008 , vol. 86, # 7 p. 668 - 675
反应条件
sodium ethanolate in ethanol T=20°C; 3 h; Inert atmosphere;
参考文献
Kikas; Carlotti; Skoric; Sindler-Kulyk; Mazzucato; Spalletti
Journal of Photochemistry and Photobiology A: Chemistry, 2012 , vol. 244, p. 38 - 46
反应条件
1.1: potassium tert-butoxide / tetrahydrofuran / 0.25 h / cooling
1.2: tetrahydrofuran / 0.58 h / cooling
2.1: NaOH / methanol; tetrahydrofuran; H2O / 3 h / 20 °C
2.2: potassium tert-butoxide / tetrahydrofuran / 3 h / 20 °C
View Scheme
参考文献
Nakamura, Tsuyoshi; Tsuji, Takashi; Iio, Yukiko; Miyazaki, Shojiro; Takemoto, Toshiyasu; Nishi, Takahide
Tetrahedron Asymmetry, 2006 , vol. 17, # 19 p. 2781 - 2792
反应条件
1.1: potassium tert-butoxide / tetrahydrofuran / 0.33 h / 20 °C
1.2: tetrahydrofuran / 0.5 h / cooling
2.1: NaOH / methanol; tetrahydrofuran; H2O / 1.5 h
2.2: potassium tert-butoxide / tetrahydrofuran / 0.83 h
View Scheme
参考文献
Tsuji, Takashi; Iio, Yukiko; Takemoto, Toshiyasu; Nishi, Takahide
Tetrahedron Asymmetry, 2005 , vol. 16, # 19 p. 3139 - 3142
