4-乙酰基苯基氨基甲酸叔丁酯合成路线 （共 11 条）
反应条件
in 1,4-dioxane T=100°C; 5 h;
参考文献
Streit, Ursula; Birbaum, Frederic; Quattropani, Anna; Bochet, Christian G.
Journal of Organic Chemistry, 2013 , vol. 78, # 14 p. 6890 - 6910
反应条件
triethylamine in 1,4-dioxane T=60°C; 6 h; Heating / reflux;
参考文献
EP1443047 A1, ;
Page 107-108 ;
反应条件
palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane T=100°C; 2.5 h;
参考文献
Qin, Lijin; Cui, Hongmeng; Zou, Dapeng; Li, Jingya; Wu, Yangjie; Zhu, Zhiwu; Wu, Yusheng
Tetrahedron Letters, 2010 , vol. 51, # 33 p. 4445 - 4448
反应条件
palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane T=100°C; 1.5 h;
参考文献
Qin, Lijin; Cui, Hongmeng; Zou, Dapeng; Li, Jingya; Wu, Yangjie; Zhu, Zhiwu; Wu, Yusheng
Tetrahedron Letters, 2010 , vol. 51, # 33 p. 4445 - 4448
反应条件
silver carbonate in ethylene glycol dimethyl ether T=80°C; 2.5 h;
参考文献
Lee, Kang-Sang; Lim, Young-Kwan; Cho, Cheon-Gyu
Tetrahedron Letters, 2002 , vol. 43, # 42 p. 7463 - 7464
反应条件
tert.-butylhydroperoxide; silver hexafluoroantimonate; [Pd(Quinox)Cl2] in dichloromethane; water T=0 - 20°C; Wacker type oxidation; Darkness;
参考文献
Michel, Brian W.; Camelio, Andrew M.; Cornell, Candace N.; Sigman, Matthew S.
Journal of the American Chemical Society, 2009 , vol. 131, p. 6076 - 6077
反应条件
methanol; tris(acetonitrile)(tricarbonyl)molybdenum T=130°C; 0.25 h; Microwave irradiationInert atmosphere; chemoselective reaction;
参考文献
Nielsen, Simon Dalsgaard; Smith, Garrick; Begtrup, Mikael; Kristensen, Jesper L.
European Journal of Organic Chemistry, 2010 , # 19 p. 3704 - 3710
反应条件
1-methylguanidine hydrochloride in ethanol Inert atmosphere;
参考文献
Organic Letters, , vol. 15, # 3 p. 646 - 649
反应条件
water T=100°C; 2.5 h;
参考文献
Chemical Communications, , # 34 p. 5144 - 5146
反应条件
ruthenium(II)-carbonyl-tris(triphenylphosphine) dihydride; 4-hydroxybutanol in ethylene glycol dimethyl ether T=115°C; 24 h; Inert atmosphere;
参考文献
Watson, Andrew J. A.; Fairbanks, Antony J.
European Journal of Organic Chemistry, 2013 , # 30 p. 6784 - 6788
