10-甲基-9-菲羧酸乙酯合成路线 (共 4 条)
反应条件
caesium carbonate; N-[2'-(dicyclohexylphosphino)-1,1'-biphenyl-2-yl]-N,N-dimethylamine; tetrakis(triphenylphosphine) palladium(0) in ethanol; toluene T=120 - 150°C; 0.166667 h; microwave irradiation;
参考文献
Young, Ha Kim; Lee, Hyuk; Yeong, Joon Kim; Bum, Tae Kim; Heo, Jung-Nyoung
Journal of Organic Chemistry, 2008 , vol. 73, # 2 p. 495 - 501
反应条件
tris(dibenzylideneacetone)dipalladium (0); cesium fluoride in acetonitrile Ambient temperature;
参考文献
Pena, Diego; Perez, Dolores; Guitian, Enrique; Castedo, Luis
Journal of the American Chemical Society, 1999 , vol. 121, # 24 p. 5827 - 5828
反应条件
1: 2,2'-dibromobiphenyl With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran T=-78°C; 1 h; 2: With anhydrous chromium(III) chloride in tetrahydrofuran T=20°C; 1 h; 3: tetrolic acid ethyl ester in tetrahydrofuran T=50°C; 24 h;
参考文献
Kanno, Ken-Ichiro; Liu, Yuanhong; Iesato, Atsushi; Nakajima, Kiyohiko; Takahashi, Tamotsu
Organic Letters, 2005 , vol. 7, # 24 p. 5453 - 5456
反应条件
bis(η3-allyl-μ-chloropalladium(II)); cesium fluoride; tris-(o-tolyl)phosphine in acetonitrile T=0 - 60°C; 3 h;
参考文献
Liu, Yi-Lin; Liang, Yun; Pi, Shao-Feng; Huang, Xiao-Cheng; Li, Jin-Heng
Journal of Organic Chemistry, 2009 , vol. 74, # 8 p. 3199 - 3202