反应条件
1: 82 percent / LiAlH4 / tetrahydrofuran / 0 °C
2: 94 percent / N-Chlorosuccinimide, dimethyl sulfide / 1.) toluene, -23 deg C, 2h; 2.) toluene, triethylamine, -23 deg C, 10 min.
3: 94 percent / n-BuLi / tetrahydrofuran / 1 h / Heating
4: 89 percent / 30percent H2O2 / methanol / 12 h / Ambient temperature
5: 70 percent / (CF3CO)2O / 72 h / Ambient temperature
6: 74 percent / NasBH4 / aq. ethanol / 12 h / Ambient temperature
7: 79 percent / vanadyl acetylacetonate, 45percent tert-butylhydroperoxide / benzene / 2 h / Heating
8: 34 percent / CrO3-2py complex / CH2Cl2 / 1.5 h / Ambient temperature
View Scheme
参考文献
Mandai, Tadakatsu; Kawada, Mikio; Otera, Junzo
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5183 - 5185
