1-苯基-3-吡啶-2-基脲合成路线 （共 19 条）
反应条件
9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; sodium t-butanolate; palladium diacetate in 1,4-dioxane
T=100°C; 2.5 h;
参考文献
Abad, Antonio; Agullo, Consuelo; Cunat, Ana Carmen; Vilanova, Cristina
Synthesis, 2005 , # 6 art. no. P13904SS, p. 915 - 924
反应条件
copper(I) oxide; tripotassium phosphate monohydrate
T=120°C; 0.666667 h; Microwave irradiationInert atmosphereNeat (no solvent);
参考文献
Gavade, Sandip; Shingare, Murlidhar; Mane, Dhananjay
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 12 p. 4167 - 4170
反应条件
copper(I) oxide; potassium tert-butylate in 1-methyl-pyrrolidin-2-one
T=100°C; 0.333333 h; Inert atmosphereMicrowave irradiation;
参考文献
Gavade, Sandip N.; Balaskar, Ravi S.; Mane, Madhav S.; Pabrekar, Pramod N.; Shingare, Murlidhar S.; Mane, Dhananjay V.
Chinese Chemical Letters, 2011 , vol. 22, # 3 p. 292 - 295
反应条件
9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; sodium t-butanolate; palladium diacetate in 1,4-dioxane
T=100°C; 2 h;
参考文献
Abad, Antonio; Agullo, Consuelo; Cunat, Ana Carmen; Vilanova, Cristina
Synthesis, 2005 , # 6 art. no. P13904SS, p. 915 - 924
反应条件
in 1,4-dioxane
1 h; Heating;
参考文献
Chien, Chia-Hui; Leung, Man-Kit; Su, Jen-Kuan; Li, Gene-Hsiang; Liu, Yi-Hung; Wang, Yu
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 1866 - 1871
反应条件
selenium; oxygen; triethylamine in toluene
T=130°C; 3 h; Autoclave;
参考文献
Zhang, Xiaopeng; Li, Desheng; Ma, Xueji; Wang, Yan; Zhang, Guisheng
Synthesis (Germany), 2013 , vol. 45, # 10 art. no. SS-2013-F0083-OP, p. 1357 - 1363
反应条件
in dimethyl sulfoxide
T=80 - 90°C; 2 h;
参考文献
Ohsawa; Arai; Igeta
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 12 p. 3570 - 3575
反应条件
phenyl N-phenylphosphoramidoazidate; triethylamine in acetonitrile
1.5 h; Heating;
参考文献
Arrieta, Ana; Palomo, Claudio
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 1-2 p. 7 - 11
反应条件
in toluene
T=70 - 95°C;
参考文献
Golobokova; Pokatilov; Proidakov; Kazantseva; Shevchenko; Vereshchagin; Kizhnyaev
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 4 p. 566 - 574
反应条件
in tetrahydrofuran
T=85°C; 2 h;
参考文献
Honma; Hayashi; Aoyama; Hashimoto; Machida; Fukasawa; Iwama; Ikeura; Ikuta; Suzuki-Takahashi; Iwasawa; Hayama; Nishimura; Morishima
Journal of Medicinal Chemistry, 2001 , vol. 44, # 26 p. 4615 - 4627
