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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
232949-65-4
合成路线
（共 10 条）
71-41-0
正戊醇
+
501-52-0
3-苯基丙酸
→
反应条件
232949-65-4
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in dichloromethane T=0 - 20°C; Esterification; 11 h;
参考文献
Kopecky, David J.; Rychnovsky, Scott D.
Journal of Organic Chemistry, 2000 , vol. 65, # 1 p. 191 - 198
638-49-3
甲酸戊酯
+
501-52-0
3-苯基丙酸
→
反应条件
232949-65-4
反应条件
tert.-butylhydroperoxide; copper(II) bis(trifluoromethanesulfonate) in 1,2-dichloro-ethane T=130°C; 12 h; Sealed tube;
参考文献
Liu, Jun; Shao, Changdong; Zhang, Yanghui; Shi, Guangfa; Pan, Shulei
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 17 p. 2637 - 2640
104-53-0
苯丙醛
+
821-09-0
4-戊烯-1-醇
→
反应条件
反应条件
potassium carbonate; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in toluene T=20°C; 12 h;
参考文献
Kiyooka, Syun-Ichi; Ueno, Mahuyu; Ishii, Eri
Tetrahedron Letters, 2005 , vol. 46, # 27 p. 4639 - 4642
71-41-0
正戊醇
+
103-25-3
3-苯丙酸甲酯
→
反应条件
232949-65-4
反应条件
potassium phosphate; N-benzyl-N,N,N-triethylammonium chloride T=20°C; 2.5 h;
参考文献
Cepanec, Ivica; Zivkovic, Andreja; Bartolincic, Anamarija; Mikuldas, Hrvoje; Litvic, Mladen; Merkas, Sonja
Croatica Chemica Acta, 2008 , vol. 81, # 3 p. 519 - 523
401587-50-6
→
反应条件
232949-65-4
反应条件
1: zinc trifluoromethanesulfonate; carbonic acid diethyl ester / 45 h / Inert atmosphere; Reflux; Solvolysis 2: Zn4O(OAc)6 / butan-1-ol / 18 h / Reflux; Inert atmosphere 3: zinc trifluoromethanesulfonate; carbonic acid diethyl ester / 45 h / 137 °C / Inert atmosphere; Solvolysis View Scheme
参考文献
Kita, Yusuke; Nishii, Yuji; Higuchi, Takafumi; Mashima, Kazushi
Angewandte Chemie - International Edition, 2012 , vol. 51, # 23 p. 5723 - 5726
1178001-75-6
→
反应条件
232949-65-4
反应条件
1: zinc trifluoromethanesulfonate; carbonic acid diethyl ester / 45 h / Inert atmosphere; Reflux; Solvolysis 2: Zn4O(OAc)6 / butan-1-ol / 18 h / Reflux; Inert atmosphere 3: zinc trifluoromethanesulfonate; carbonic acid diethyl ester / 45 h / 137 °C / Inert atmosphere; Solvolysis View Scheme
参考文献
Kita, Yusuke; Nishii, Yuji; Higuchi, Takafumi; Mashima, Kazushi
Angewandte Chemie - International Edition, 2012 , vol. 51, # 23 p. 5723 - 5726
1156900-68-3
→
反应条件
232949-65-4
反应条件
1: zinc trifluoromethanesulfonate; carbonic acid diethyl ester / 45 h / Inert atmosphere; Reflux; Solvolysis 2: Zn4O(OAc)6 / butan-1-ol / 18 h / Reflux; Inert atmosphere 3: zinc trifluoromethanesulfonate; carbonic acid diethyl ester / 45 h / 137 °C / Inert atmosphere; Solvolysis View Scheme
参考文献
Kita, Yusuke; Nishii, Yuji; Higuchi, Takafumi; Mashima, Kazushi
Angewandte Chemie - International Edition, 2012 , vol. 51, # 23 p. 5723 - 5726
20627-49-0
→
反应条件
232949-65-4
反应条件
1: Zn4O(OAc)6 / butan-1-ol / 18 h / Reflux; Inert atmosphere 2: zinc trifluoromethanesulfonate; carbonic acid diethyl ester / 45 h / 137 °C / Inert atmosphere; Solvolysis View Scheme
参考文献
Kita, Yusuke; Nishii, Yuji; Higuchi, Takafumi; Mashima, Kazushi
Angewandte Chemie - International Edition, 2012 , vol. 51, # 23 p. 5723 - 5726
91564-20-4
→
反应条件
232949-65-4
反应条件
1: zinc trifluoromethanesulfonate; carbonic acid diethyl ester / 45 h / Inert atmosphere; Reflux; Solvolysis 2: Zn4O(OAc)6 / butan-1-ol / 18 h / Reflux; Inert atmosphere 3: zinc trifluoromethanesulfonate; carbonic acid diethyl ester / 45 h / 137 °C / Inert atmosphere; Solvolysis View Scheme
参考文献
Kita, Yusuke; Nishii, Yuji; Higuchi, Takafumi; Mashima, Kazushi
Angewandte Chemie - International Edition, 2012 , vol. 51, # 23 p. 5723 - 5726
71-41-0
正戊醇
+
51816-46-7
→
反应条件
232949-65-4
反应条件
zinc trifluoromethanesulfonate; carbonic acid diethyl ester T=137°C; 45 h; Inert atmosphereSolvolysis;
参考文献
Kita, Yusuke; Nishii, Yuji; Higuchi, Takafumi; Mashima, Kazushi
Angewandte Chemie - International Edition, 2012 , vol. 51, # 23 p. 5723 - 5726
