苯并[e][1]苯并二硫杂环戊烷合成路线 (共 24 条)
反应条件
1: 98 percent / NaOH / ethanol; H2O / 6 h / Heating
2: 54 percent / powdered copper / quinoline / 5 h / Heating
3: 50 percent / HI, red P / H2O / 2 h / Heating
View Scheme
参考文献
Sidorenko, T. N.; Terent'eva, G. A.; Andrienko, O. S.; Savinykh, Yu. V.; Aksenov, V. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , p. 156 - 160
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 2 p. 192 - 196
反应条件
1: trifluorormethanesulfonic acid / chlorobenzene / 3 h / Reflux
2: chloranil / toluene / 24 h / Reflux
View Scheme
参考文献
Rungtaweevoranit, Bunyarat; Butsuri, Akkarapol; Wongma, Krittaphat; Sadorn, Karoon; Neranon, Kitjanit; Nerungsi, Chakkrapan; Thongpanchang, Tienthong
Tetrahedron Letters, 2012 , vol. 53, # 14 p. 1816 - 1818
参考文献
Campaigne; Cline
Journal of Organic Chemistry, 1956 , vol. 21, p. 32,35
反应条件
acetic acid; zinc
Erhitzen des Reaktionsprodukts mit Tetrachlor-<1,4>benzochinon in Xylol;
参考文献
Mayer
Justus Liebigs Annalen der Chemie, 1931 , vol. 488, p. 259,275
Full Text Show Details
Carruthers
Journal of the Chemical Society, 1953 , p. 4186
反应条件
tetrahydrofuran; lithium aluminium tetrahydride
参考文献
Davies; Porter
Journal of the Chemical Society, 1957 , p. 4967,4969
反应条件
1: acetic acid
2: lithium alanate; tetrahydrofuran
View Scheme
参考文献
Davies; Porter
Journal of the Chemical Society, 1957 , p. 4967,4969
反应条件
1: potassium hydroxide; toluene
2: acetic acid
3: lithium alanate; tetrahydrofuran
View Scheme
参考文献
Davies; Porter
Journal of the Chemical Society, 1957 , p. 4967,4969
反应条件
1: ethanolic sodium ethylate
2: tin (IV)-chloride; chloroform
View Scheme
参考文献
Banfield et al.
Journal of the Chemical Society, 1956 , p. 2603,2607
反应条件
T=900°C; P=0.02 Torr; 2.77778E-06 h; Product distribution;
参考文献
Ibrahim, Yehia A; Al-Awadi, Nouria A; Kaul, Kamini
Tetrahedron, 2001 , vol. 57, # 34 p. 7377 - 7381
参考文献
Davies; Porter
Journal of the Chemical Society, 1957 , p. 4967,4969