苯并[e][1]苯并二硫杂环戊烷合成路线 (共 24 条)
反应条件
aluminium trichloride in 1,2-dichloro-ethane
Ambient temperature;
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1143 - 1148
反应条件
1: 70 percent / AlCl3 / 1,2-dichloro-ethane / Ambient temperature
2: 83 percent / zinc dust, conc. ammonium hydroxide / Heating
View Scheme
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1143 - 1148
反应条件
1: 70 percent / AlCl3 / 1,2-dichloro-ethane / Ambient temperature
2: 83 percent / zinc dust, conc. ammonium hydroxide / Heating
3: 79 percent / LiAlH4 / diethyl ether
View Scheme
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1143 - 1148
反应条件
1: 70 percent / AlCl3 / 1,2-dichloro-ethane / Ambient temperature
2: 83 percent / zinc dust, conc. ammonium hydroxide / Heating
3: 79 percent / LiAlH4 / diethyl ether
4: 79 percent / CrO3 / pyridine
View Scheme
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1143 - 1148