in hexane dissoloving Re2(CO)9(NCCH3) (0.157 mmol) and CH3C2CO2CH3 (0.236 mmol) in hexane; heating to reflux for 8 h; cooling;; removal of solvent by evapn.; sepn. of residue by thin layer chromy.; elution with hexane/CH2Cl2 (4:1); elem. anal.;;
参考文献
Adams, Richard D.; Chen, Linfeng; Wu, Wengan
Organometallics, 1993 , vol. 12, p. 1257 - 1265
Hamper, Bruce C.; Leschinsky, Kindrick L.; Massey, Steven S.; Bell, Crystal L.; Brannigan, Lawrence H.; Prosch, S. Douglas
Journal of Agricultural and Food Chemistry, 1995 , vol. 43, # 1 p. 219 - 228