1: tri-ruthenium(0)dodecacarbonyl; 1,3-bis-(diphenylphosphino)propane; 3,5-dimethyl-benzoic acid / toluene / 24 h / 120 °C / |Sealed tube; |Inert atmosphere
2: toluene-4-sulfonic acid / toluene / 2 h / 85 °C
View Scheme
参考文献
Geary, Laina M.; Chen, Te-Yu; Montgomery, T. Patrick; Krische, Michael J.
Journal of the American Chemical Society, 2014 , vol. 136, # 16 p. 5920 - 5922
1: sodium tetrahydroborate / methanol / 0 °C
2: tri-ruthenium(0)dodecacarbonyl; 1,3-bis-(diphenylphosphino)propane; 3,5-dimethyl-benzoic acid / toluene / 24 h / 120 °C / |Sealed tube; |Inert atmosphere
3: toluene-4-sulfonic acid / toluene / 2 h / 85 °C
View Scheme
参考文献
Geary, Laina M.; Chen, Te-Yu; Montgomery, T. Patrick; Krische, Michael J.
Journal of the American Chemical Society, 2014 , vol. 136, # 16 p. 5920 - 5922