5-氰基-二甲基异邻苯二甲酸酯合成路线 (共 3 条)
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=60°C; 72 h;
参考文献
MEDIVIR AB
Patent: WO2008/119772 A1, 2008 ;
Location in patent: Page/Page column 72 ;
WO 2008/119772 A1
反应条件
3,5-dimethyl pyridine in diethyl ether
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 438 - 446
反应条件
1: With methanol; sodium hydroxide; water in tetrahydrofuran T=20°C; 17 h; 2: With hydrogenchloride; water in ethyl acetate
参考文献
MEDIVIR AB
Patent: WO2008/119772 A1, 2008 ;
Location in patent: Page/Page column 72-73 ;
WO 2008/119772 A1