2-溴-3,4,5-三甲氧基苯甲酸合成路线 （共 21 条）
反应条件
ammonium hydroxide; copper
参考文献
Mayer; Fikentscher
Chemische Berichte, 1956 , vol. 89, p. 511,517
反应条件
1: butyl lithium; diethyl ether / -75 °C / anschliessend Einleiten von CO2 2: phosphorus (V)-oxide / 200 °C View Scheme
参考文献
Friedrich; Mirbach
Chemische Berichte, 1959 , vol. 92, p. 2751,2754
参考文献
Friedrich; Mirbach
Chemische Berichte, 1959 , vol. 92, p. 2574,2575, 2577
参考文献
Michalsky,J.; Smrz,M.
Monatshefte fuer Chemie, 1960 , vol. 91, p. 307 - 312
反应条件
copper in methanol
18 h; Heating;
参考文献
AMAZENTIS SA; RINSCH, Christopher, L.; BLANCO-BOSE, William; SCHNEIDER, Bernard; MOUCHIROUD, Laurent; RYU, Dongryeol; ANDREUX, Penelope; AUWERX, Johan
Patent: WO2014/4902 A2, 2014 ;
Location in patent: Sheet 35 ;
反应条件
1: aqueous NaOH; copper-powder
2: alkaline aqueous solution
View Scheme
参考文献
Mayer; Fikentscher
Chemische Berichte, 1956 , vol. 89, p. 511,517
反应条件
n-butyllithium; diethyl ether
T=-75°C; anschliessend Einleiten von CO2;
参考文献
Friedrich; Mirbach
Chemische Berichte, 1959 , vol. 92, p. 2751,2754
反应条件
1: 11 percent / acetone / 2 h
2: 2,4,6-trichloro-s-triazine
View Scheme
参考文献
Beugelmans, Rene; Ginsburg, Helene; Bois-Choussy, Michele
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1149 - 1152
反应条件
1: aqueous NaOH; copper-powder
2: AlBr3; benzene
3: aqueous HCl
View Scheme
参考文献
Mayer; Fikentscher
Chemische Berichte, 1956 , vol. 89, p. 511,517
反应条件
sodium hydroxide; copper
参考文献
Mayer; Fikentscher
Chemische Berichte, 1958 , vol. 91, p. 1536,1540
