(R)-(-)-1,2,3,4-四氢-1-萘酚合成路线 (共 59 条)
反应条件
borane-THF; (S)-oxazaborolidine in tetrahydrofuran T=0°C; 0.0833333 h;
参考文献
Sarvary, Ian; Almqvist, Fredrik; Frejd, Torbjoern
Chemistry - A European Journal, 2001 , vol. 7, # 10 p. 2158 - 2166
反应条件
1: With benzo[1,3,2]dioxaborole; rhodium complex 2 in toluene T=20°C; Addition; Hydroboration; 2 h; 2: With sodium hydroxide; water; dihydrogen peroxide in toluene T=20°C; Oxidation; 2 h;
参考文献
Doucet, Henri; Fernandez, Elena; Layzell, Timothy P.; Brown, John M.
Chemistry - A European Journal, 1999 , vol. 5, # 4 p. 1320 - 1330
反应条件
sodium carbonate in toluene T=40°C; 72 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 23, # 11-12 p. 828 - 833
反应条件
in water T=25°C; 72 h; by Helminthosporium species;
参考文献
Canadian Journal of Chemistry, , vol. 65, p. 502 - 507
反应条件
sodium carbonate in toluene T=40°C; 72 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Merabet-Khelassi, Mounia; Houiene, Zahia; Aribi-Zouioueche, Louisa; Riant, Olivier
Tetrahedron Asymmetry, 2012 , vol. 23, # 11-12 p. 828 - 833
反应条件
sodium hydroxide; (R)-1-(2-diphenylphosphino-1-naphthyl)phenanthridine rhodium; dihydrogen peroxide; benzo[1,3,2]dioxaborole 1.) THF, RT, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron: Asymmetry, , vol. 6, # 10 p. 2593 - 2596
反应条件
dimethylsulfide borane complex in tetrahydrofuran T=20°C; 2 h; enantioselective reaction;
参考文献
Hosoda, Naoya; Kamito, Hideaki; Takano, Miki; Takebe, Yoshitaka; Yamaguchi, Yoshitaka; Asami, Masatoshi
Tetrahedron, 2013 , vol. 69, # 11 p. 2509 - 2509
反应条件
[bis(acetoxy)iodo]benzene; tetraethylammonium bromide; [Mn{CHCH2CHPhNCH[OC6H2(t-Bu)2]}2]Cl in water T=20°C; 1 h;
参考文献
Angewandte Chemie - International Edition, , vol. 42, # 9 p. 1042 - 1044
反应条件
Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 37, # 37 p. 6777 - 6780
反应条件
in water T=25°C; 72 h; by Helminthosporium species; Yield given;
参考文献
Holland, Herbert L.; Bergen, Eleanor J.; Chenchaiah, P. Chinna; Khan, Shaheer H.; Munoz, Benito; et al.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 502 - 507