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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
23357-51-9
合成路线
（共 12 条）
23357-51-9
→
反应条件
65915-64-2
+
53732-47-1
(S)-(+)-1,2,3,4-四氢-1-萘酚
+
21503-12-8
+
23357-45-1
(R)-(-)-1,2,3,4-四氢-1-萘酚
反应条件
tris(hydroxymethyl)methylamine hydrochloride; sodium chloride; calcium chloride in water; acetonitrile T=25°C; pH=8; 96 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Zheng, Gao-Wei; Liu, Xu-Yun; Zhang, Zhi-Jun; Tian, Ping; Lin, Guo-Qiang; Xu, Jian-He
RSC Advances, 2013 , vol. 3, # 43 p. 20446 - 20449
23357-51-9
→
反应条件
53732-47-1
(S)-(+)-1,2,3,4-四氢-1-萘酚
+
23357-45-1
(R)-(-)-1,2,3,4-四氢-1-萘酚
反应条件
in water hydrolysis by a Rhizopus nigricans culture; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kasai, Masaji; Kawai, Ken-ichi; Imuta, Mitsuru; Ziffer, Herman
Journal of Organic Chemistry, 1984 , vol. 49, # 4 p. 675 - 679
23357-51-9
→
反应条件
53732-47-1
(S)-(+)-1,2,3,4-四氢-1-萘酚
反应条件
2: K2CO3 / methanol / Ambient temperature View Scheme
参考文献
Laumen, Kurt; Schneider, Manfred P.
Journal of the Chemical Society, Chemical Communications, 1988 , p. 598 - 600
23357-51-9
→
反应条件
447-53-0
1,2-二氢萘
反应条件
T=450°C;
参考文献
Alder; Wolff
Justus Liebigs Annalen der Chemie, 1952 , vol. 576, p. 182,205
23357-51-9
→
反应条件
65915-64-2
+
23357-45-1
(R)-(-)-1,2,3,4-四氢-1-萘酚
反应条件
sodium carbonate in toluene T=40°C; 72 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 23, # 11-12 p. 828 - 833
23357-51-9
→
反应条件
65915-64-2
+
21503-12-8
+
23357-45-1
(R)-(-)-1,2,3,4-四氢-1-萘酚
反应条件
sodium carbonate in toluene T=40°C; 72 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Merabet-Khelassi, Mounia; Houiene, Zahia; Aribi-Zouioueche, Louisa; Riant, Olivier
Tetrahedron Asymmetry, 2012 , vol. 23, # 11-12 p. 828 - 833
23357-51-9
→
反应条件
23357-45-1
(R)-(-)-1,2,3,4-四氢-1-萘酚
反应条件
phosphate buffer; lipase T=20°C;
参考文献
Laumen, Kurt; Schneider, Manfred P.
Journal of the Chemical Society, Chemical Communications, 1988 , p. 598 - 600
23357-51-9
→
反应条件
65915-64-2
+
53732-47-1
(S)-(+)-1,2,3,4-四氢-1-萘酚
+
21503-12-8
+
23357-45-1
(R)-(-)-1,2,3,4-四氢-1-萘酚
反应条件
tris(hydroxymethyl)methylamine hydrochloride; sodium chloride; calcium chloride in water; acetonitrile T=25°C; pH=8; 96 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Zheng, Gao-Wei; Liu, Xu-Yun; Zhang, Zhi-Jun; Tian, Ping; Lin, Guo-Qiang; Xu, Jian-He
RSC Advances, 2013 , vol. 3, # 43 p. 20446 - 20449
23357-51-9
→
反应条件
53732-47-1
(S)-(+)-1,2,3,4-四氢-1-萘酚
+
23357-45-1
(R)-(-)-1,2,3,4-四氢-1-萘酚
反应条件
in water hydrolysis by a Rhizopus nigricans culture; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kasai, Masaji; Kawai, Ken-ichi; Imuta, Mitsuru; Ziffer, Herman
Journal of Organic Chemistry, 1984 , vol. 49, # 4 p. 675 - 679
23357-51-9
→
反应条件
529-33-9
1,2,3,4-四氢-1-萘酚
反应条件
[t-Bu2SnOH(Cl)]2 in methanol Deacetylation; 12 h; Heating;
参考文献
Orita, Akihiro; Hamada, Yuuki; Nakano, Takehiko; Toyoshima, Shinji; Otera, Junzo
Chemistry - A European Journal, 2001 , vol. 7, # 15 p. 3321 - 3327
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