苯并[g][1]苯并二硫杂环戊烷合成路线 (共 42 条)
反应条件
1: 70 percent / aq. HCl, HCl gas / 2 h / 65 - 70 °C
2: 90 percent / LiAlH4 / diethyl ether / 4 h / Ambient temperature
View Scheme
参考文献
Tedjamulia, Marvin L.; Stuart, John G.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 1215 - 1219
反应条件
n-butyllithium
1.) ether, -20 deg C, 1 h, 2.) room temperature, 4 h, 3.) 25 deg C, 16 h;; Yield given. Multistep reaction;
参考文献
Tedjamulia, Marvin L.; Stuart, John G.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 1215 - 1219