N-(苯甲酸基)丁二酰亚胺合成路线 (共 46 条)
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in N,N-dimethyl-formamide T=20°C; 0.166667 h;
参考文献
Fujisaki, Fumiko; Oishi, Marumi; Sumoto, Kunihiro
Chemical and Pharmaceutical Bulletin, 2007 , vol. 55, # 1 p. 124 - 127
反应条件
N'-(3-dimethylaminopropyl)-N-ethylcarbodiimide in N,N-dimethyl-formamide T=0 - 20°C; Esterification;
参考文献
Colton, Ian J.; Anderson, Janelle R.; Gao, Jinming; Chapman, Robert G.; Isaacs, Lyle; Whitesides, George M.
Journal of the American Chemical Society, 1997 , vol. 119, # 52 p. 12701 - 12709
反应条件
palladium diacetate; triethylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in dimethyl sulfoxide T=70°C; P=760 Torr; 17 h;
参考文献
Lou, Rongliang; VanAlstine, Melissa; Sun, Xufeng; Wentland, Mark P.
Tetrahedron Letters, 2003 , vol. 44, # 12 p. 2477 - 2480
反应条件
[bis(acetoxy)iodo]benzene in ethyl acetate 0.5 h; cooling;
参考文献
Wang, Naiwei; Liu, Renhua; Xu, Qing; Liang, Xinmiao
Chemistry Letters, 2006 , vol. 35, # 6 p. 566 - 567
反应条件
palladium diacetate; triethylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in dimethyl sulfoxide T=70°C; P=760 Torr; 17 h;
参考文献
Lou, Rongliang; VanAlstine, Melissa; Sun, Xufeng; Wentland, Mark P.
Tetrahedron Letters, 2003 , vol. 44, # 12 p. 2477 - 2480
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in ethyl acetate T=20 - 70°C; 12 h;
参考文献
Tan, Bin; Toda, Narihiro; Barbas III, Carlos F.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12538 - 12541
Angew. Chem., 2012 , vol. 124, # 50 p. 12706 - 12709,4
反应条件
triethylamine in N,N-dimethyl-formamide T=20°C; 0.5 h;
参考文献
Bailen, Miguel A; Chinchilla, Rafael; Dodsworth, David J; Najera, Carmen
Tetrahedron Letters, 2002 , vol. 43, # 9 p. 1661 - 1664
反应条件
palladium diacetate; triethylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in dimethyl sulfoxide T=70°C; P=760 Torr; 17 h;
参考文献
Lou, Rongliang; VanAlstine, Melissa; Sun, Xufeng; Wentland, Mark P.
Tetrahedron Letters, 2003 , vol. 44, # 12 p. 2477 - 2480
反应条件
1-hydroxy-pyrrolidine-2,5-dione; oxygen; [Co(O2CCH3)2]*4H2O; sodium hydrogencarbonate in acetonitrile T=20°C; P=760.051 Torr; 1 h; Molecular sieve;
参考文献
Chemistry - An Asian Journal, , vol. 7, # 7 p. 1542 - 1545
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide T=20°C; 16 h;
参考文献
Angewandte Chemie - International Edition, , vol. 41, # 21 p. 4059 - 4061