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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
23405-48-3
合成路线
（共 22 条）
100-68-5
茴香硫醚
+
98-88-4
苯甲酰氯
→
反应条件
23405-48-3
反应条件
bismuth trifluoromethanesulphonate T=80°C; Friedel-Crafts acylation; 0.5 h; Ionic liquid;
参考文献
Tran, Phuong Hoang; Duus, Fritz; Le, Thach Ngoc
Tetrahedron Letters, 2012 , vol. 53, # 2 p. 222 - 224
104-95-0
4-溴硫代苯甲醚
+
63468-90-6
→
反应条件
23405-48-3
反应条件
quinoline; 1,10-phenanthroline; tris-(o-tolyl)phosphine; copper(I) bromide in 1-methyl-pyrrolidin-2-one; quinoline T=170°C; 16 h;
参考文献
Goossen, Lukas J.; Rudolphi, Felix; Oppel, Christoph; Rodriguez, Nuria
Angewandte Chemie - International Edition, 2008 , vol. 47, # 16 p. 3043 - 3045
100-68-5
茴香硫醚
+
93-97-0
苯甲酸酐
→
反应条件
23405-48-3
反应条件
Yb[C(SO2(C4H9)3)3]3 in various solvent(s) T=150°C; Friedel-Crafts acylation; 20 h;
参考文献
Barrett, Anthony G. M.; Bouloc, Nathalie; Braddock, D. Christopher; Chadwick, David; Henderson, David A.
Synlett, 2002 , # 10 p. 1653 - 1656
90-90-4
4-溴苯甲酰苯
+
67-68-5
二甲基亚砜
→
反应条件
23405-48-3
反应条件
copper(l) iodide; zinc diacetate T=135°C; 36 h; regioselective reaction;
参考文献
Joseph, P.J. Amal; Priyadarshini; Kantam, M. Lakshmi; Sreedhar
Tetrahedron, 2013 , vol. 69, # 38 p. 8276 - 8283
100-68-5
茴香硫醚
+
98-88-4
苯甲酰氯
→
反应条件
23405-48-3
+
1620-95-7
反应条件
copper(II) bis(trifluoromethanesulfonate) in 1,2-dichloro-ethane T=80°C; Friedel-Crafts benzoylation; 12 h;
参考文献
Hoangtran, Phuong; Bichle Do, Ngoc; Ngocle, Thach
Tetrahedron Letters, 2014 , vol. 55, # 1 p. 205 - 208
104-95-0
4-溴硫代苯甲醚
+
98-88-4
苯甲酰氯
→
反应条件
23405-48-3
反应条件
1: 1-bromo-4-methylsulfanyl benzene With diisobutyl-aluminum chloride; diisobutylaluminium hydride; magnesium; lithium chloride in tetrahydrofuran; n-heptane T=25°C; 2: benzoyl chloride With CuCN*2LiCl in tetrahydrofuran; n-heptane T=-10 - 25°C; 3 h;
参考文献
Gao, Hongjun; Knochel, Paul
Synlett, 2009 , # 8 p. 1321 - 1325
90-90-4
4-溴苯甲酰苯
+
74-88-4
甲基碘
→
反应条件
23405-48-3
反应条件
1: (4-bromophenyl)(phenyl)methanone With potassium tert-butylate; thiolacetic acid potassium salt in dimethyl sulfoxide 3 h; Irradiation; 2: methyl iodide in water; dimethyl sulfoxide
参考文献
Schmidt, Luciana C.; Rey, Valentina; Penenory, Alicia B.
European Journal of Organic Chemistry, 2006 , # 9 p. 2210 - 2214
1442-06-4
4-(甲硫基)苯甲酰氯
+
71-43-2
苯
→
反应条件
23405-48-3
反应条件
AlCl3, aluminium chloride Friedel Crafts acylation;
参考文献
Gabbutt, Christopher D.; Heron, B. Mark; Kolla, Suresh B.; Kilner, Colin; Coles, Simon J.; Horton, Peter N.; Hursthouse, Michael B.
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 17 p. 3096 - 3104
90-90-4
4-溴苯甲酰苯
+
74-88-4
甲基碘
→
反应条件
119-61-9
二苯甲酮
+
23405-48-3
反应条件
1: (4-bromophenyl)(phenyl)methanone With potassium tert-butylate; thiourea in dimethyl sulfoxide 3 h; UV-irradiation; 2: methyl iodide in water; dimethyl sulfoxide
参考文献
Argueello, Juan E.; Schmidt, Luciana C.; Penenory, Alicia B.
Organic Letters, 2003 , vol. 5, # 22 p. 4133 - 4136
17302-63-5
甲基硫醚阴离子
+
90-90-4
4-溴苯甲酰苯
→
反应条件
23405-48-3
反应条件
N(Et)4ClO4 in acetonitrile Rate constant;
参考文献
Amatore; Pinson; Saveant; Thiebault
Journal of the American Chemical Society, 1982 , vol. 104, # 3 p. 817 - 826
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