6-甲基-1,3-苯并噁唑-2-硫醇合成路线 (共 2 条)
反应条件
thionyl chloride; N,N-dimethyl-formamide T=0°C; 1 h;
参考文献
PIERRE FABRE MEDICAMENT; Dupont-Passelaigue, Elisabeth; Le Roy, Isabelle; Pignier, Christophe
Patent: US2013/172326 A1, 2013 ;
Location in patent: Paragraph 0089; 0090 ;
反应条件
sodium hydroxide in ethanol; water
4 h; Ambient temperature;
参考文献
Schickaneder, Helmut; Engler, Heidrun; Szelenyi, Istvan
Journal of Medicinal Chemistry, 1987 , vol. 30, # 3 p. 547 - 551