反应条件
1.1: chloro-trimethyl-silane / tetrahydrofuran / 0.25 h / |Inert atmosphere; |Sealed tube 1.2: 57 °C / |Inert atmosphere; |Sealed tube 2.1: 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; bis(dibenzylideneacetone)-palladium(0) / tetrahydrofuran / 3 h / 65 °C / |Inert atmosphere; |Sealed tube View Scheme
参考文献
Wong, Brian; Linghu, Xin; Crawford, James J.; Drobnick, Joy; Lee, Wendy; Zhang, Haiming
Tetrahedron, 2014 , vol. 70, # 7 p. 1508 - 1515