1-(4-溴苯基)-3-羟基-1H-吡唑合成路线 （共 3 条）
反应条件
FeCl3·6H2O in N,N-dimethyl-formamide T=80°C; 16 h;
参考文献
Li, Yuhao; Liu, Rui; Yan, Zhangwei; Zhang, Xiangning; Zhu, Hongjun
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 11 p. 3341 - 3347
反应条件
1: sodium methylate / ethanol; toluene / 16 h / 40 - 45 °C 2: FeCl3·6H2O / N,N-dimethyl-formamide / 16 h / 80 °C View Scheme
参考文献
Li, Yuhao; Liu, Rui; Yan, Zhangwei; Zhang, Xiangning; Zhu, Hongjun
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 11 p. 3341 - 3347
反应条件
1.1: hydrogenchloride; sodium nitrite / water / 0.33 h / Cooling with ice 1.2: 2 h / -10 - -5 °C 2.1: sodium methylate / ethanol; toluene / 16 h / 40 - 45 °C 3.1: FeCl3·6H2O / N,N-dimethyl-formamide / 16 h / 80 °C View Scheme
参考文献
Li, Yuhao; Liu, Rui; Yan, Zhangwei; Zhang, Xiangning; Zhu, Hongjun
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 11 p. 3341 - 3347
