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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-苯基-2-丁醇
合成路线
（共 214 条）
2344-70-9
4-苯基-2-丁醇
→
反应条件
2550-26-7
苄基丙酮
+
2344-70-9
4-苯基-2-丁醇
反应条件
nicotinamide adenine dinucleotide phosphate; tris(hydroxymethyl)methylamine hydrochloride; acetone in cyclohexane; water T=50°C; 24 h;
参考文献
Kunisu, Takashi; Oguma, Takuya; Katsuki, Tsutomu
Journal of the American Chemical Society, 2011 , vol. 133, # 33 p. 12937 - 12939
108-05-4
醋酸乙烯酯
+
2344-70-9
4-苯基-2-丁醇
→
反应条件
10415-88-0
乙酸-(4-苯基)-2-丁酯
+
2344-70-9
4-苯基-2-丁醇
反应条件
50 U aminoacylase E.C. 3.5.1.14 in hexane Acetylation; 168 h;
参考文献
Bakker; Spruijt; Van Rantwijk; Sheldon
Tetrahedron Asymmetry, 2000 , vol. 11, # 8 p. 1801 - 1808
2344-70-9
4-苯基-2-丁醇
→
反应条件
22374-89-6
1-甲基-3-苯基丙胺
反应条件
tri-ruthenium(0)dodecacarbonyl; ammonia; N-phenyl-2-(dicyclohexylphosphino)pyrrol in 1,1-dimethylpropan-1-ol T=150°C; 20 h; Cooling with dry iceMolecular sieve; chemoselective reaction;
参考文献
Imm, Sebastian; Neubert, Lorenz; Neumann, Helfried; Beller, Matthias
Angewandte Chemie - International Edition, 2010 , vol. 49, # 44 p. 8126 - 8129
2344-70-9
4-苯基-2-丁醇
→
反应条件
2550-26-7
苄基丙酮
+
22374-89-6
1-甲基-3-苯基丙胺
反应条件
alanine dehydrogenase; (S)-α-alanine; pyridoxal 5'-phosphate; nicotinamide adenine dinucleotide; ammonium chloride; alcohol dehydrogenase in aq. phosphate buffer T=20°C; 24 h; Enzymatic reaction; Reagent/catalyst;
参考文献
Chemistry - A European Journal, , vol. 19, # 12 p. 4030 - 4035
2344-70-9
4-苯基-2-丁醇
→
反应条件
13030-26-7
反应条件
1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione in 1,2-dichloro-ethane T=40°C; 9 h; Irradiation;
参考文献
Furuyama, Shusuke; Togo, Hideo
Synlett, 2010 , # 15 p. 2325 - 2329
5344-90-1
邻氨基苯甲醇
+
2344-70-9
4-苯基-2-丁醇
→
反应条件
1613-41-8
反应条件
potassium hydroxide; dodec-1-ene; tris(triphenylphosphine)ruthenium(II) chloride in 1,4-dioxane T=80°C; 20 h;
参考文献
Cho, Chan Sik; Kim, Bok Tae; Choi, Heung-Jin; Kim, Tae-Jeong; Shim, Sang Chul
Tetrahedron, 2003 , vol. 59, # 40 p. 7997 - 8002
2344-70-9
4-苯基-2-丁醇
→
反应条件
143097-80-7
反应条件
chloro-trimethyl-silane; lithium bromide in acetonitrile 86 h; Heating;
参考文献
Crosignani, Stefano; Nadal, Brice; Li, Zhengning; Linclau, Bruno
Chemical Communications, 2003 , # 2 p. 260 - 261
2344-70-9
4-苯基-2-丁醇
→
反应条件
143097-80-7
+
132665-55-5
反应条件
2,6-dimethylpyridine; tetraethylammonium bromide; Xtalfluor-E® in dichloromethane T=21°C; Inert atmosphere;
参考文献
Pouliot, Marie-France; Mahe, Olivier; Hamel, Jean-Denys; Desroches, Justine; Paquin, Jean-Francois
Organic Letters, 2012 , vol. 14, # 21 p. 5428 - 5431,4
2344-70-9
4-苯基-2-丁醇
→
反应条件
6683-51-8
反应条件
potassium tert-butylate; C29H30ClNOP2Ru(1+) in acetone T=60°C; 1 h; Inert atmosphere; Product distribution / selectivity;
参考文献
TAKASAGO INTERNATIONAL CORPORATION; TOUGE, Taichiro; AOKI, Kunie; NARA, Hideki; KURIYAMA, Wataru
Patent: WO2012/144650 A1, 2012 ;
Location in patent: Page/Page column 46-48 ;
2344-70-9
4-苯基-2-丁醇
→
反应条件
4489-84-3
+
6683-51-8
反应条件
1.1: triphenylphosphine; 1H-imidazole; bromine / dichloromethane / 27 h / 20 °C / |Inert atmosphere 2.1: potassium carbonate / acetone / 24 h / |Reflux; |Inert atmosphere 3.1: (NH4)6[Mo7O24]*4H2O; dihydrogen peroxide / methanol; water / 2.5 h / 0 - 20 °C / |Inert atmosphere 4.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / |Inert atmosphere 4.2: 20 h / 20 °C / |Inert atmosphere 5.1: N,N,N',N,-tetramethylethylenediamine; iron (III) acetylacetonate; CPME / diethyl ether / 18 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Denmark, Scott E.; Cresswell, Alexander J.
Journal of Organic Chemistry, 2013 , vol. 78, # 24 p. 12593 - 12628
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