in diethyl ether
Me3SiCH2Cl added to a suspn. of excess lithium in Et2O at -23°C,vigorously stirred for 2,5 h, Me3GeCl added; warmed to room temp.; diluted (Et2O); washed satd. soln. of NH4Cl; dried over Na2SO4; solvent evapd.; distd.;
参考文献
Barton, Thomas J.; Hoekman, S. Kent
Journal of the American Chemical Society, 1980 , vol. 102, # 5 p. 1584 - 1591