2-氨基-5-甲基苯硫酚合成路线 （共 55 条）
反应条件
1: 86 percent / potassium hydroxide / methanol / 24 h 2: 65 percent / triethylamine / acetonitrile / standing overnight 3: potassium hydroxide / ethanol / 1.5 h / Heating 4: H2O / Schotten-Baumann 5: potassium hydroxide / ethanol / 3 h / 180 °C / sealed tube View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, p. 317 - 326
Zhurnal Organicheskoi Khimii, , vol. 23, # 2 p. 355 - 365
参考文献
DE370854 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 915
DE399909 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 1048
反应条件
in der Kalischmelze;
参考文献
Chemische Berichte, , vol. 22, p. 1066
反应条件
bei der Kalischmelze;
参考文献
Chemische Berichte, , vol. 22, p. 1066
反应条件
triethylamine in diethyl ether T=20°C; 1 h;
参考文献
Drozd, V.N.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 317 - 326
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 355 - 365
反应条件
1: 59 percent / triethylamine / diethyl ether / 0.25 h 2: 76 percent / triethylamine / diethyl ether / 1 h / 20 °C View Scheme
参考文献
Drozd, V.N.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 317 - 326
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 355 - 365
反应条件
1: zinc 2: KMnO4 View Scheme
参考文献
Fridman
Zhurnal Obshchei Khimii, 1950 , vol. 20, p. 1191,1195; engl. Ausg. S. 1235, 1239
反应条件
polyphosphoric acid T=220°C;
参考文献
Tzanopoulou, Stamatia; Sagnou, Marina; Paravatou-Petsotas, Maria; Gourni, Eleni; Loudos, George; Xanthopoulos, Stavros; Lafkas, Daniel; Kiaris, Hippokratis; Varvarigou, Alexandra; Pirmettis, Ioannis C.; Papadopoulos, Minas; Pelecanou, Maria
Journal of Medicinal Chemistry, 2010 , vol. 53, # 12 p. 4633 - 4641
参考文献
Fridman
Zhurnal Obshchei Khimii, 1950 , vol. 20, p. 1191,1195; engl. Ausg. S. 1235, 1239
反应条件
potassium carbonate in N,N-dimethyl-formamide T=110 - 120°C; 8 h;
参考文献
Mashraqui, Sabir H.; Biswas, Maloyesh M.; Nivalkar, Kishor R.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1996 , vol. 35, # 10 p. 1031 - 1037
