2-氨基-5-甲基苯硫酚合成路线 （共 55 条）
反应条件
triethylamine in diethyl ether
0.25 h;
参考文献
Drozd, V.N.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 317 - 326
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 355 - 365
反应条件
1: 59 percent / triethylamine / diethyl ether / 0.25 h
2: 76 percent / triethylamine / diethyl ether / 1 h / 20 °C
3: 86 percent / potassium hydroxide / methanol / 24 h
4: 65 percent / triethylamine / acetonitrile / standing overnight
View Scheme
参考文献
Drozd, V.N.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 317 - 326
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 355 - 365
反应条件
oxygen in dimethyl sulfoxide; chlorobenzene
T=140°C; P=760.051 Torr; 16 h; Sealed tube;
参考文献
Liao, Yunfeng; Qi, Hongrui; Chen, Shanping; Jiang, Pengcheng; Zhou, Wang; Deng, Guo-Jun
Organic Letters, 2012 , vol. 14, # 23 p. 6004 - 6007
反应条件
1: 59 percent / triethylamine / diethyl ether / 0.25 h
2: 80 percent / triethylamine / diethyl ether / standing overnight
View Scheme
参考文献
Drozd, V.N.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 317 - 326
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 355 - 365
参考文献
Hess
Chemische Berichte, 1881 , vol. 14, p. 489
反应条件
1: zinc
2: KMnO4
3: SOCl2
View Scheme
参考文献
Fridman
Zhurnal Obshchei Khimii, 1950 , vol. 20, p. 1191,1195; engl. Ausg. S. 1235, 1239
反应条件
0.05 h; microwave irradiation;
参考文献
Khairnar, Bhikan J; Salunke, Rahul S; Patil, Premchand B; Patil, Sanjay A; Kapade, Rajeshwar J; Girase, Pravin S; Chaudhari, Bhata R
E-Journal of Chemistry, 2012 , vol. 9, # 1 p. 318 - 322
反应条件
aluminum oxide in chloroform
0.1 h; microwave irradiation;
参考文献
Paul; Gupta; Loupy; Rani; Dandia
Synthetic Communications, 2001 , vol. 31, # 5 p. 711 - 717
反应条件
piperidine in tetrahydrofuran
2 h; Reflux;
参考文献
Khairnar, Bhikan J.; Girase, Pravin S.; Chaudhari
Oriental Journal of Chemistry, 2013 , vol. 29, # 1 p. 285 - 289
反应条件
1: hydrazine hydrate; N,N-dimethyl-formamide / 0.01 h / Neat (no solvent); Microwave irradiation
2: 0.05 h / 30 °C / Neat (no solvent); Microwave irradiation
View Scheme
参考文献
Kalwania; Chomal; Choudhary, Savita
Asian Journal of Chemistry, 2011 , vol. 23, # 11 p. 5133 - 5136
