2-氨基-5-甲基苯硫酚合成路线 (共 55 条)
反应条件
0.0333333 h; microwave irradiation;
参考文献
Dandia, Anshu; Sarawgi, Pritima; Hursthouse, Michael B.; Bingham, Ann L.; Light, Mark E.; Drake, John E.; Ratnani, Raju
Journal of Chemical Research, 2006 , # 7 p. 445 - 448
反应条件
sodium hydroxide in ethanol; water
T=10°C;
参考文献
Ingle; Sawale; Mane
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 2 p. 124 - 128
反应条件
aluminum oxide in chloroform
0.116667 h; microwave irradiation;
参考文献
Paul; Gupta; Loupy; Rani; Dandia
Synthetic Communications, 2001 , vol. 31, # 5 p. 711 - 717
反应条件
in diethyl ether
Ambient temperature;
参考文献
Gupta; Gautam; Kumar
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 1 p. 171 - 174
反应条件
hydrogenchloride in ethanol
3 h; Heating;
参考文献
Singh, S. P.; Prakash, Indra; Tomer, R. K.; Prakash, O. M.; Sawhney, S. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 1 p. 37 - 42
反应条件
2: K2cr2O7; aqueous H2SO4; HCl
View Scheme
参考文献
Fridman
Zhurnal Obshchei Khimii, 1950 , vol. 20, p. 1807,1811; engl. Ausg. S. 1871, 1874, 1875
反应条件
toluene-4-sulfonic acid
T=120°C; 5 h; Green chemistry;
参考文献
Vidavalur, Siddaiah; Gajula, Mahaboob Basha; Tadikonda, Ramu; Nakka, Mangarao; Dega, Sudhakar; Yadav, Santosh Kumar; Voosala, Christopher
Tetrahedron Letters, 2014 , vol. 55, # 16 p. 2691 - 2694
反应条件
in neat (no solvent)
0.5 h; Green chemistry; Time;
参考文献
Yoon, Soon Byung; Chun, Eun Jeong; Noh, Young Ri; Yoon, Yong Jin; Lee, Sang-Geyong
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 9 p. 2819 - 2821
参考文献
Jacobson; Ney
Chemische Berichte, 1889 , vol. 22, p. 909,910
Justus Liebigs Annalen der Chemie, 1893 , vol. 277, p. 232,234
反应条件
palladium diacetate; triethylamine; triphenylphosphine in tetrahydrofuran
T=100 - 110°C; P=20686.5 Torr; 60 h; Autoclave;
参考文献
Troisi, Luigino; Granito, Catia; Perrone, Serena; Rosato, Francesca
Tetrahedron Letters, 2011 , vol. 52, # 33 p. 4330 - 4332