4,4-二甲基-2-氧戊醛合成路线 （共 4 条）
参考文献
Wright, Stephen W.; Harris, Richard R.; Kerr, Janet S.; Green, Alicia M.; Pinto, Donald J.; et al.
Journal of Medicinal Chemistry, 1992 , vol. 35, # 22 p. 4061 - 4068
反应条件
ethanol; sodium hydride in tert-butyl methyl ether T=20°C; Claisen condensation; 1.66667 h; Inert atmosphereReflux;
参考文献
Bertogg, Andreas; Hintermann, Lukas; Huber, Dominique P.; Perseghini, Mauro; Sanna, Maria; Togni, Antonio
Helvetica Chimica Acta, 2012 , vol. 95, # 3 p. 353 - 403
反应条件
ethanol; hydrazine hydrate in methanol; tert-butyl methyl ether T=50 - 80°C; 2 h; Inert atmosphere;
参考文献
Bertogg, Andreas; Hintermann, Lukas; Huber, Dominique P.; Perseghini, Mauro; Sanna, Maria; Togni, Antonio
Helvetica Chimica Acta, 2012 , vol. 95, # 3 p. 353 - 403
反应条件
2-azido-1-ethylpyridin-1-ium fluoroborate; sodium acetate in methanol; water
1.16667 h; Ambient temperature; Yields of byproduct given;
参考文献
Sezer, Oezkan; Anac, Olcay
Helvetica Chimica Acta, 1994 , vol. 77, # 8 p. 2323 - 2334
